methyl 4-[[4-[(methylphenylamino)methyl]phenyl]methoxy]benzenepropanoate

Base Information

Chemical Name:methyl 4-[[4-[(methylphenylamino)methyl]phenyl]methoxy]benzenepropanoate
CAS No.:691902-23-5
Molecular Formula:C₂₅H₂₇NO₃
Molecular Weight:389.494
Hs Code.:

Synonyms:methyl 4-[[4-[(methylphenylamino)methyl]phenyl]methoxy]benzenepropanoate

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Chemical Property of methyl 4-[[4-[(methylphenylamino)methyl]phenyl]methoxy]benzenepropanoate

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Technology Process of methyl 4-[[4-[(methylphenylamino)methyl]phenyl]methoxy]benzenepropanoate

There total 2 articles about methyl 4-[[4-[(methylphenylamino)methyl]phenyl]methoxy]benzenepropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 691904-73-1
methyl 3-(4-(4-(bromomethyl)benzyloxy)phenyl)propanoate

: 100-61-8
N-methylaniline

: 691902-23-5
methyl 4-[[4-[(methylphenylamino)methyl]phenyl]methoxy]benzenepropanoate

Guidance literature:: N-methylaniline; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

methyl 3-(4-(4-(bromomethyl)benzyloxy)phenyl)propanoate; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

Reference yield:

: 623-24-5
1,4-bis(bromomethyl)benzene

: 5597-50-2
3-(4-hydroxyphenyl)propionic acid methyl ester

: 691902-23-5
methyl 4-[[4-[(methylphenylamino)methyl]phenyl]methoxy]benzenepropanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetone / 8 h / Heating / reflux

2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

2.2: 3 h / 20 °C

With sodium hydride; potassium carbonate; In N,N-dimethyl-formamide; acetone;