N-tritylaspartic acid α-(2-mercaptopyridyl)-β-cyclohexyl diester

Base Information

Chemical Name:N-tritylaspartic acid α-(2-mercaptopyridyl)-β-cyclohexyl diester
CAS No.:151012-00-9
Molecular Formula:C₃₄H₃₄N₂O₃S
Molecular Weight:550.722
Hs Code.:

Synonyms:N-tritylaspartic acid α-(2-mercaptopyridyl)-β-cyclohexyl diester

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Chemical Property of N-tritylaspartic acid α-(2-mercaptopyridyl)-β-cyclohexyl diester

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Technology Process of N-tritylaspartic acid α-(2-mercaptopyridyl)-β-cyclohexyl diester

There total 3 articles about N-tritylaspartic acid α-(2-mercaptopyridyl)-β-cyclohexyl diester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 2637-34-5,73018-10-7
2-Sulfanylpyridine

: 151036-42-9
N^α-trityl-L-aspartic acid β-cyclohexyl ester

: 151012-00-9
N-tritylaspartic acid α-(2-mercaptopyridyl)-β-cyclohexyl diester

Guidance literature:: With dicyclohexyl-carbodiimide; In ethyl acetate; at 0 - 20 ℃;
DOI:10.1021/jm9508043

Reference yield:

: 73821-95-1
Boc-Asp(O-cyclohexyl)-OH

: 151012-00-9
N-tritylaspartic acid α-(2-mercaptopyridyl)-β-cyclohexyl diester

Guidance literature:: Multi-step reaction with 3 steps

1: TFA / CH₂Cl₂ / 0.75 h / Ambient temperature

2: 1.) Me₃SiCl, Et₃N, 2.) MeOH

3: 83 percent / DCC / ethyl acetate / 0 - 20 °C

With methanol; chloro-trimethyl-silane; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; ethyl acetate;
DOI:10.1021/jm9508043

Reference yield:

: 112259-66-2
β-cyclohexyl L-aspartate

: 151012-00-9
N-tritylaspartic acid α-(2-mercaptopyridyl)-β-cyclohexyl diester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Me₃SiCl, Et₃N, 2.) MeOH

2: 83 percent / DCC / ethyl acetate / 0 - 20 °C

With methanol; chloro-trimethyl-silane; triethylamine; dicyclohexyl-carbodiimide; In ethyl acetate;
DOI:10.1021/jm9508043