p-methoxyphenyl 3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-glucopyranosyl-(1->4)-3-O-acetyl-6-O-benzyl-2-acetylamino-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:p-methoxyphenyl 3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-glucopyranosyl-(1->4)-3-O-acetyl-6-O-benzyl-2-acetylamino-2-deoxy-β-D-glucopyranoside
CAS No.:1279722-05-2
Molecular Formula:C₃₆H₄₄N₄O₁₅
Molecular Weight:772.763
Hs Code.:

Synonyms:p-methoxyphenyl 3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-glucopyranosyl-(1->4)-3-O-acetyl-6-O-benzyl-2-acetylamino-2-deoxy-β-D-glucopyranoside

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Chemical Property of p-methoxyphenyl 3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-glucopyranosyl-(1->4)-3-O-acetyl-6-O-benzyl-2-acetylamino-2-deoxy-β-D-glucopyranoside

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Technology Process of p-methoxyphenyl 3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-glucopyranosyl-(1->4)-3-O-acetyl-6-O-benzyl-2-acetylamino-2-deoxy-β-D-glucopyranoside

There total 4 articles about p-methoxyphenyl 3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-glucopyranosyl-(1->4)-3-O-acetyl-6-O-benzyl-2-acetylamino-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1241376-04-4
3,4,6-tri-O-acetyl-2-azido-2-deoxy-D-glucopyranosyl ortho-(hex-1-ynyl)benzoate

: 1279722-05-2
p-methoxyphenyl 3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-glucopyranosyl-(1->4)-3-O-acetyl-6-O-benzyl-2-acetylamino-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoromethanesulfonyloxy(triphenylphosphine)gold(I) / diethyl ether / -30 - 20 °C / Inert atmosphere; Molecular sieve

2: ethylenediamine / ethanol / 14 h / 100 °C

3: pyridine; dmap / 20 °C

With pyridine; dmap; trifluoromethanesulfonyloxy(triphenylphosphine)gold(I); ethylenediamine; In diethyl ether; ethanol;
DOI:10.1002/cbic.201000561

Reference yield:

: 1185868-59-0
C₄₂H₄₄N₄O₁₆

: 1279722-05-2
p-methoxyphenyl 3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-glucopyranosyl-(1->4)-3-O-acetyl-6-O-benzyl-2-acetylamino-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: ethylenediamine / ethanol / 14 h / 100 °C

2: pyridine; dmap / 20 °C

With pyridine; dmap; ethylenediamine; In ethanol;
DOI:10.1002/cbic.201000561

Reference yield:

: 1140972-41-3
C₃₀H₂₉NO₉

: 1279722-05-2
p-methoxyphenyl 3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-glucopyranosyl-(1->4)-3-O-acetyl-6-O-benzyl-2-acetylamino-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoromethanesulfonyloxy(triphenylphosphine)gold(I) / diethyl ether / -30 - 20 °C / Inert atmosphere; Molecular sieve

2: ethylenediamine / ethanol / 14 h / 100 °C

3: pyridine; dmap / 20 °C

With pyridine; dmap; trifluoromethanesulfonyloxy(triphenylphosphine)gold(I); ethylenediamine; In diethyl ether; ethanol;
DOI:10.1002/cbic.201000561