1-(O³-acetyl-O⁵-benzoyl-2-fluoro-β-D-2-deoxy-arabinofuranosyl)-1H-pyrimidine-2,4-dione

Base Information

• Chemical Name: 1-(O³-acetyl-O⁵-benzoyl-2-fluoro-β-D-2-deoxy-arabinofuranosyl)-1H-pyrimidine-2,4-dione
• CAS No.: 69124-02-3
• Molecular Formula: C₁₈H₁₇FN₂O₇
• Molecular Weight: 392.341

Synonyms:1-(O³-acetyl-O⁵-benzoyl-2-fluoro-β-D-2-deoxy-arabinofuranosyl)-1H-pyrimidine-2,4-dione

Chemical Property of 1-(O³-acetyl-O⁵-benzoyl-2-fluoro-β-D-2-deoxy-arabinofuranosyl)-1H-pyrimidine-2,4-dione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(O³-acetyl-O⁵-benzoyl-2-fluoro-β-D-2-deoxy-arabinofuranosyl)-1H-pyrimidine-2,4-dione

There total 2 articles about 1-(O³-acetyl-O⁵-benzoyl-2-fluoro-β-D-2-deoxy-arabinofuranosyl)-1H-pyrimidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-di-O-acetyl-5-O-benzoyl-2-deoxy-2-fluoro-D-arabinofuranosyl bromide (56632-81-6) + uracil (66-22-8,144104-68-7,18324-22-6,27072-01-1,2920-92-5,51953-19-6) + O,O'-bis-(trimethylsilyl)uracil (10457-14-4) → 1-(O3-acetyl-O5-benzoyl-2-fluoro-β-D-2-deoxy-arabinofuranosyl)-1H-pyrimidine-2,4-dione (69124-02-3)

Guidance literature:

With ammonium sulfate; In methanol; hexamethyldisilazan; dichloromethane;

Reference yield:

→ 1-(O3-acetyl-O5-benzoyl-2-fluoro-β-D-2-deoxy-arabinofuranosyl)-1H-pyrimidine-2,4-dione (69124-02-3)

Guidance literature:

3-O-acetyl-5-O-benzoyl-2-deoxy-2-fluor-β-D-1-brom-arabinose, 2,4-Bis-<(trimethylsilyl)oxy>-pyrimidin;

DOI:10.1021/jm00187a005

Reference yield:

1-(O3-acetyl-O5-benzoyl-2-fluoro-β-D-2-deoxy-arabinofuranosyl)-1H-pyrimidine-2,4-dione (69124-02-3) → fialuridine (69123-98-4)

Guidance literature:

With iodine; In methanolic ammonia; diethyl ether; acetic acid;

upstream raw materials:

1,3-di-O-acetyl-5-O-benzoyl-2-deoxy-2-fluoro-D-arabinofuranosyl bromide

uracil

O,O'-bis-(trimethylsilyl)uracil

Downstream raw materials:

1-(2-deoxy-2-fluoro-β-D-arabinofuranosyl)-5-bromouracil

fialuridine

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