benzyl 4-(4-(2-(3-hydroxybutylamino)-2-oxoethyloxy)phenyl)butylcarbamate

Base Information

Chemical Name:benzyl 4-(4-(2-(3-hydroxybutylamino)-2-oxoethyloxy)phenyl)butylcarbamate
CAS No.:960398-60-1
Molecular Formula:C₂₄H₃₂N₂O₅
Molecular Weight:428.528
Hs Code.:

Synonyms:benzyl 4-(4-(2-(3-hydroxybutylamino)-2-oxoethyloxy)phenyl)butylcarbamate

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Chemical Property of benzyl 4-(4-(2-(3-hydroxybutylamino)-2-oxoethyloxy)phenyl)butylcarbamate

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Technology Process of benzyl 4-(4-(2-(3-hydroxybutylamino)-2-oxoethyloxy)phenyl)butylcarbamate

There total 1 articles about benzyl 4-(4-(2-(3-hydroxybutylamino)-2-oxoethyloxy)phenyl)butylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 960398-59-8
benzyl 4-(4-(2-(3-(tert-butyldimethylsilyloxy)butylamino)-2-oxoethyloxy)phenyl)butylcarbamate

: 960398-60-1
benzyl 4-(4-(2-(3-hydroxybutylamino)-2-oxoethyloxy)phenyl)butylcarbamate

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 72h;

Reference yield: 71.0%

: 960398-60-1
benzyl 4-(4-(2-(3-hydroxybutylamino)-2-oxoethyloxy)phenyl)butylcarbamate

: 960398-61-2
benzyl 4-(4-(2-oxo-2-(3-oxobutylamino)ethoxy)phenyl)butylcarbamate

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃;

Reference yield:

: 960398-60-1
benzyl 4-(4-(2-(3-hydroxybutylamino)-2-oxoethyloxy)phenyl)butylcarbamate

: 960398-63-4
(R)-2-(4-(4-aminobutyl)phenoxy)-N-(3-(2-(4-(benzyloxy)-3-formamidophenyl)-2-hydroxyethylamino)butyl)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridinium chlorochromate / dichloromethane / 20 °C

2.1: methanol / 3 h / 20 °C

2.2: 20 °C

3.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C / 760.05 Torr

With hydrogen; pyridinium chlorochromate; palladium 10% on activated carbon; In methanol; dichloromethane;