benzyl 4-(4-(2-(3-(tert-butyldimethylsilyloxy)butylamino)-2-oxoethyloxy)phenyl)butylcarbamate

Base Information

Chemical Name:benzyl 4-(4-(2-(3-(tert-butyldimethylsilyloxy)butylamino)-2-oxoethyloxy)phenyl)butylcarbamate
CAS No.:960398-59-8
Molecular Formula:C₃₀H₄₆N₂O₅Si
Molecular Weight:542.791
Hs Code.:

Synonyms:benzyl 4-(4-(2-(3-(tert-butyldimethylsilyloxy)butylamino)-2-oxoethyloxy)phenyl)butylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 4-(4-(2-(3-(tert-butyldimethylsilyloxy)butylamino)-2-oxoethyloxy)phenyl)butylcarbamate

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Technology Process of benzyl 4-(4-(2-(3-(tert-butyldimethylsilyloxy)butylamino)-2-oxoethyloxy)phenyl)butylcarbamate

There total 2 articles about benzyl 4-(4-(2-(3-(tert-butyldimethylsilyloxy)butylamino)-2-oxoethyloxy)phenyl)butylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 847201-23-4
2-(4-(4-(benzyloxycarbonylamino)butyl)phenoxy)acetic acid

: 763932-62-3
3-(t-butyldimethylsilylhydroxy)butylamine

: 960398-59-8
benzyl 4-(4-(2-(3-(tert-butyldimethylsilyloxy)butylamino)-2-oxoethyloxy)phenyl)butylcarbamate

Guidance literature:: With 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 960398-58-7
benzyl 3-(tert-butyldimethylsilyloxy)butylcarbamate

: 960398-59-8
benzyl 4-(4-(2-(3-(tert-butyldimethylsilyloxy)butylamino)-2-oxoethyloxy)phenyl)butylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / ethanol / 5 h

2: 1,1'-carbonyldiimidazole / tetrahydrofuran / 20 °C

With hydrogen; 1,1'-carbonyldiimidazole; palladium 10% on activated carbon; In tetrahydrofuran; ethanol;