ethyl 3-amino-1-[2'-hydroxy-3'-(methyloxy)-4-biphenylyl]-1H-pyrrole-2-carboxylate hydrochloride

Base Information

Chemical Name:ethyl 3-amino-1-[2'-hydroxy-3'-(methyloxy)-4-biphenylyl]-1H-pyrrole-2-carboxylate hydrochloride
CAS No.:1346607-53-1
Molecular Formula:C₂₀H₂₀N₂O₄*ClH
Molecular Weight:388.851
Hs Code.:

Synonyms:ethyl 3-amino-1-[2'-hydroxy-3'-(methyloxy)-4-biphenylyl]-1H-pyrrole-2-carboxylate hydrochloride

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Chemical Property of ethyl 3-amino-1-[2'-hydroxy-3'-(methyloxy)-4-biphenylyl]-1H-pyrrole-2-carboxylate hydrochloride

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Technology Process of ethyl 3-amino-1-[2'-hydroxy-3'-(methyloxy)-4-biphenylyl]-1H-pyrrole-2-carboxylate hydrochloride

There total 1 articles about ethyl 3-amino-1-[2'-hydroxy-3'-(methyloxy)-4-biphenylyl]-1H-pyrrole-2-carboxylate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 259209-17-1
[2-hydroxy-3-(methyloxy)phenyl]boronic acid

: 1272673-95-6
ethyl 3-amino-1-(4-bromophenyl)-1H-pyrrole-2-carboxylate hydrochloride

: 1346607-53-1
ethyl 3-amino-1-[2'-hydroxy-3'-(methyloxy)-4-biphenylyl]-1H-pyrrole-2-carboxylate hydrochloride

Guidance literature:: [2-hydroxy-3-(methyloxy)phenyl]boronic acid; ethyl 3-amino-1-(4-bromophenyl)-1H-pyrrole-2-carboxylate hydrochloride; With caesium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; water; for 2h; Reflux;

With hydrogenchloride; In 1,4-dioxane; water;

Reference yield: 82.0%

: 16744-98-2
1-Fluoro-2-isocyanato-benzene

: 1346607-53-1
ethyl 3-amino-1-[2'-hydroxy-3'-(methyloxy)-4-biphenylyl]-1H-pyrrole-2-carboxylate hydrochloride

: 1346607-63-3
ethyl 3-({[(2-fluorophenyl)amino]carbonyl}amino)-1-[2'-hydroxy-3'-(methyloxy)-4-biphenylyl]-1H-pyrrole-2-carboxylate

Guidance literature:: In toluene; for 48h; Reflux;

Reference yield:

: 462-08-8
pyridin-3-ylamine

: 1346607-53-1
ethyl 3-amino-1-[2'-hydroxy-3'-(methyloxy)-4-biphenylyl]-1H-pyrrole-2-carboxylate hydrochloride

: 1346608-16-9
5-[2'-hydroxy-3'-(methyloxy)-4-biphenylyl]-3-(3-pyridinyl)-1H-pyrrolo[3,2-d]pyrimidine-2,4(3H,5H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 3 h / 20 °C

1.2: 80 °C

2.1: ethanol; sodium / 80 °C

With ethanol; sodium; In dichloromethane;