(C₆H₅)3PAuS₂CNC₄H₈NH₂⁽¹⁺⁾*BF₄^(1-)=(C₆H₅)3PAuS₂CNC₄H₈NH₂BF₄

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Chemical Name:(C₆H₅)3PAuS₂CNC₄H₈NH₂⁽¹⁺⁾*BF₄^(1-)=(C₆H₅)3PAuS₂CNC₄H₈NH₂BF₄
CAS No.:1165801-04-6
Molecular Formula:BF₄*C₂₃H₂₅AuN₂PS₂
Molecular Weight:708.342
Hs Code.:

(C<sub>6</sub>H<sub>5</sub>)3PAuS<sub>2</sub>CNC<sub>4</sub>H<sub>8</sub>NH<sub>2</sub><sup>(1+)</sup>*BF<sub>4</sub><sup>(1-)</sup>=(C<sub>6</sub>H<sub>5</sub>)3PAuS<sub>2</sub>CNC<sub>4</sub>H<sub>8</sub>NH<sub>2</sub>BF<sub>4</sub>

Synonyms:(C₆H₅)3PAuS₂CNC₄H₈NH₂⁽¹⁺⁾*BF₄^(1-)=(C₆H₅)3PAuS₂CNC₄H₈NH₂BF₄

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Chemical Property of (C₆H₅)3PAuS₂CNC₄H₈NH₂⁽¹⁺⁾*BF₄^(1-)=(C₆H₅)3PAuS₂CNC₄H₈NH₂BF₄

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Technology Process of (C₆H₅)3PAuS₂CNC₄H₈NH₂⁽¹⁺⁾*BF₄^(1-)=(C₆H₅)3PAuS₂CNC₄H₈NH₂BF₄

There total 1 articles about (C₆H₅)3PAuS₂CNC₄H₈NH₂⁽¹⁺⁾*BF₄^(1-)=(C₆H₅)3PAuS₂CNC₄H₈NH₂BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 13755-29-8
sodium tetrafluoroborate

: 99-00-3
piperazine-1-carbodithioic acid

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 1165801-04-6
(C₆H₅)3PAuS₂CNC₄H₈NH₂⁽¹⁺⁾*BF₄^(1-)=(C₆H₅)3PAuS₂CNC₄H₈NH₂BF₄

Guidance literature:: In methanol; dichloromethane; byproducts: NaCl; (aerobic conditions); addn. of a soln. of ligand and NaBF4 in methanol to a soln. of gold complex in CH2Cl2, stirring for 2 h in the dark; evapn., addn. of acetone, filtration through diatomaceous earth, evapn.,trituration in Et2O, washing with Et2O, drying, recrystn. (CH2Cl2/ethan ol); elem. anal.;
DOI:10.1021/ic802442d

Reference yield: 90.0%

: 75-15-0,12122-00-8
carbon disulfide

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 1165801-04-6
(C₆H₅)3PAuS₂CNC₄H₈NH₂⁽¹⁺⁾*BF₄^(1-)=(C₆H₅)3PAuS₂CNC₄H₈NH₂BF₄

: 1165801-05-7
((C₆H₅)3PAu)2S₂CNC₄H₈NCS₂

Guidance literature:: With triethylamine; In dichloromethane; acetone; (aerobic conditions); addn. of amine and CS2 to a soln. of gold complex in acetone, addn. of a soln. of gold chloride complex in CH2Cl2, stirring for 1 h; evapn., addn. of Et2O, trituration in a sonic bath, filtration, washing with water, ethanol, hexane, recrystn. (CH2Cl2/ethanol); elem. anal.;
DOI:10.1021/ic802442d