[Ph(acetonitrile)Pt((2,6-Me₂C₆H₃)-N=C(Me)-C(Me)=N-(2,6-Me₂C₆H₃))][BF₄]

Base Information

• Chemical Name: [Ph(acetonitrile)Pt((2,6-Me₂C₆H₃)-N=C(Me)-C(Me)=N-(2,6-Me₂C₆H₃))][BF₄]
• CAS No.: 312925-36-3
• Molecular Formula: BF₄*C₂₈H₃₂N₃Pt
• Molecular Weight: 692.467

Synonyms:[Ph(acetonitrile)Pt((2,6-Me₂C₆H₃)-N=C(Me)-C(Me)=N-(2,6-Me₂C₆H₃))][BF₄]

Chemical Property of [Ph(acetonitrile)Pt((2,6-Me₂C₆H₃)-N=C(Me)-C(Me)=N-(2,6-Me₂C₆H₃))][BF₄]

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of [Ph(acetonitrile)Pt((2,6-Me₂C₆H₃)-N=C(Me)-C(Me)=N-(2,6-Me₂C₆H₃))][BF₄]

There total 3 articles about [Ph(acetonitrile)Pt((2,6-Me₂C₆H₃)-N=C(Me)-C(Me)=N-(2,6-Me₂C₆H₃))][BF₄] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

tetrafluoroboric acid diethyl ether (67969-82-8) + Ph2Pt((2,6-Me2C6H3)-N=C(Me)-C(Me)=N-(2,6-Me2C6H3)) (312925-30-7) + acetonitrile (75-05-8,26809-02-9) → [Ph(acetonitrile)Pt((2,6-Me2C6H3)-N=C(Me)-C(Me)=N-(2,6-Me2C6H3))][BF4] (312925-36-3)

Guidance literature:

In dichloromethane; to a soln. of complex in CH2Cl2 and CH3CN was added a 54% soln. of HBF4in Et2O, the mixt. was stirred for 30 min; the solvent was removed, the residue was washed with Et2O, dried in vac.; elem. anal.;

DOI:10.1021/ja0017460

Reference yield:

N,N'-bis(2,6-dimethylphenyl)butane-2,3-diimine (49673-40-7) → [Ph(acetonitrile)Pt((2,6-Me2C6H3)-N=C(Me)-C(Me)=N-(2,6-Me2C6H3))][BF4] (312925-36-3)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene

2: acetonitrile

In toluene; acetonitrile;

DOI:10.1021/ja056694z

Reference yield:

cis-(PtPh2(SMe2)2) → [Ph(acetonitrile)Pt((2,6-Me2C6H3)-N=C(Me)-C(Me)=N-(2,6-Me2C6H3))][BF4] (312925-36-3)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene

2: acetonitrile

In toluene; acetonitrile;

DOI:10.1021/ja056694z

upstream raw materials:

tetrafluoroboric acid diethyl ether

Ph₂Pt((2,6-Me₂C₆H₃)-N=C(Me)-C(Me)=N-(2,6-Me₂C₆H₃))

acetonitrile

N,N'-bis(2,6-dimethylphenyl)butane-2,3-diimine

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