(S)-2-(N-(3-(benzyldisulfanyl)-5-(2-(6-methoxynaphthalen-2-yl)propanoyloxy)pent-2-en-2-yl)formamido)acetic acid

Base Information

Chemical Name:(S)-2-(N-(3-(benzyldisulfanyl)-5-(2-(6-methoxynaphthalen-2-yl)propanoyloxy)pent-2-en-2-yl)formamido)acetic acid
CAS No.:1333480-99-1
Molecular Formula:C₂₉H₃₁NO₆S₂
Molecular Weight:553.7
Hs Code.:

Synonyms:(S)-2-(N-(3-(benzyldisulfanyl)-5-(2-(6-methoxynaphthalen-2-yl)propanoyloxy)pent-2-en-2-yl)formamido)acetic acid

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Chemical Property of (S)-2-(N-(3-(benzyldisulfanyl)-5-(2-(6-methoxynaphthalen-2-yl)propanoyloxy)pent-2-en-2-yl)formamido)acetic acid

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Technology Process of (S)-2-(N-(3-(benzyldisulfanyl)-5-(2-(6-methoxynaphthalen-2-yl)propanoyloxy)pent-2-en-2-yl)formamido)acetic acid

There total 12 articles about (S)-2-(N-(3-(benzyldisulfanyl)-5-(2-(6-methoxynaphthalen-2-yl)propanoyloxy)pent-2-en-2-yl)formamido)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.9%

: 1333480-96-8
(S)-4-(N-(2-tert-butoxy-2-oxoethyl)formamido)-3-(benzyldisulfanyl)pent-3-enyl 2-(6-methoxynaphthalen-2-yl)propanoate

: 1333480-99-1
(S)-2-(N-(3-(benzyldisulfanyl)-5-(2-(6-methoxynaphthalen-2-yl)propanoyloxy)pent-2-en-2-yl)formamido)acetic acid

Guidance literature:: With perchloric acid; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.ejmech.2011.05.029

Reference yield:

: 1333480-94-6
(S)-4-(N-(2-tert-butoxy-2-oxoethyl)formamido)-3-(ethyldisulfanyl)pent-3-enyl 2-(6-methoxynaphthalen-2-yl)propanoate

: 1333480-99-1
(S)-2-(N-(3-(benzyldisulfanyl)-5-(2-(6-methoxynaphthalen-2-yl)propanoyloxy)pent-2-en-2-yl)formamido)acetic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: perchloric acid / dichloromethane / 1 h / 20 °C / Inert atmosphere

2.1: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 0.5 h

2.2: 60 °C

3.1: trifluoroacetic acid / dichloromethane / 1.5 h / 0 °C

4.1: water / methanol / 1 h / 37 °C / pH 7.4 / aq. phosphate buffer; Enzymatic reaction

5.1: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C

6.1: perchloric acid / dichloromethane / 1 h / 20 °C / Inert atmosphere

With dmap; perchloric acid; water; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.ejmech.2011.05.029

Reference yield:

: 1333480-98-0
(S)-2-(N-(3-(isopropyldisulfanyl)-5-(2-(6-methoxynaphthalen-2-yl)propanoyloxy)pent-2-en-2-yl)formamido)acetic acid

: 1333480-99-1
(S)-2-(N-(3-(benzyldisulfanyl)-5-(2-(6-methoxynaphthalen-2-yl)propanoyloxy)pent-2-en-2-yl)formamido)acetic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 0.5 h

1.2: 60 °C

2.1: trifluoroacetic acid / dichloromethane / 1.5 h / 0 °C

3.1: water / methanol / 1 h / 37 °C / pH 7.4 / aq. phosphate buffer; Enzymatic reaction

4.1: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C

5.1: perchloric acid / dichloromethane / 1 h / 20 °C / Inert atmosphere

With dmap; perchloric acid; water; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.ejmech.2011.05.029