(S)-4-(N-(2-tert-butoxy-2-oxoethyl)formamido)-3-(benzyldisulfanyl)pent-3-enyl 2-(6-methoxynaphthalen-2-yl)propanoate

Base Information

Chemical Name:(S)-4-(N-(2-tert-butoxy-2-oxoethyl)formamido)-3-(benzyldisulfanyl)pent-3-enyl 2-(6-methoxynaphthalen-2-yl)propanoate
CAS No.:1333480-96-8
Molecular Formula:C₃₃H₃₉NO₆S₂
Molecular Weight:609.808
Hs Code.:

Synonyms:(S)-4-(N-(2-tert-butoxy-2-oxoethyl)formamido)-3-(benzyldisulfanyl)pent-3-enyl 2-(6-methoxynaphthalen-2-yl)propanoate

Suppliers and Price of (S)-4-(N-(2-tert-butoxy-2-oxoethyl)formamido)-3-(benzyldisulfanyl)pent-3-enyl 2-(6-methoxynaphthalen-2-yl)propanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-4-(N-(2-tert-butoxy-2-oxoethyl)formamido)-3-(benzyldisulfanyl)pent-3-enyl 2-(6-methoxynaphthalen-2-yl)propanoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-4-(N-(2-tert-butoxy-2-oxoethyl)formamido)-3-(benzyldisulfanyl)pent-3-enyl 2-(6-methoxynaphthalen-2-yl)propanoate

There total 12 articles about (S)-4-(N-(2-tert-butoxy-2-oxoethyl)formamido)-3-(benzyldisulfanyl)pent-3-enyl 2-(6-methoxynaphthalen-2-yl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.4%

: 1333480-93-5
tert-butyl 2-(N-(3-(benzyldisulfanyl)-5-hydroxypent-2-en-2-yl)formamido)acetate

: 22204-53-1
(2S)-2-(6-methoxy(2-naphthyl))propanoic acid

: 1333480-96-8
(S)-4-(N-(2-tert-butoxy-2-oxoethyl)formamido)-3-(benzyldisulfanyl)pent-3-enyl 2-(6-methoxynaphthalen-2-yl)propanoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/j.ejmech.2011.05.029

Reference yield:

: 1333480-94-6
(S)-4-(N-(2-tert-butoxy-2-oxoethyl)formamido)-3-(ethyldisulfanyl)pent-3-enyl 2-(6-methoxynaphthalen-2-yl)propanoate

: 1333480-96-8
(S)-4-(N-(2-tert-butoxy-2-oxoethyl)formamido)-3-(benzyldisulfanyl)pent-3-enyl 2-(6-methoxynaphthalen-2-yl)propanoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: perchloric acid / dichloromethane / 1 h / 20 °C / Inert atmosphere

2.1: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 0.5 h

2.2: 60 °C

3.1: trifluoroacetic acid / dichloromethane / 1.5 h / 0 °C

4.1: water / methanol / 1 h / 37 °C / pH 7.4 / aq. phosphate buffer; Enzymatic reaction

5.1: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C

With dmap; perchloric acid; water; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.ejmech.2011.05.029

Reference yield:

: 1333480-95-7
(S)-4-(N-(2-tert-butoxy-2-oxoethyl)formamido)-3-(isopropyldisulfanyl)pent-3-enyl 2-(6-methoxynaphthalen-2-yl)propanoate

: 1333480-96-8
(S)-4-(N-(2-tert-butoxy-2-oxoethyl)formamido)-3-(benzyldisulfanyl)pent-3-enyl 2-(6-methoxynaphthalen-2-yl)propanoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: perchloric acid / dichloromethane / 1 h / 20 °C / Inert atmosphere

2.1: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 0.5 h

2.2: 60 °C

3.1: trifluoroacetic acid / dichloromethane / 1.5 h / 0 °C

4.1: water / methanol / 1 h / 37 °C / pH 7.4 / aq. phosphate buffer; Enzymatic reaction

5.1: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C

With dmap; perchloric acid; water; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.ejmech.2011.05.029