L-BocAlaGly 4-iodophenylamide

Base Information

Chemical Name:L-BocAlaGly 4-iodophenylamide
CAS No.:1072115-75-3
Molecular Formula:C₁₆H₂₂IN₃O₄
Molecular Weight:447.273
Hs Code.:

Synonyms:L-BocAlaGly 4-iodophenylamide

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Chemical Property of L-BocAlaGly 4-iodophenylamide

Chemical Property:

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Technology Process of L-BocAlaGly 4-iodophenylamide

There total 4 articles about L-BocAlaGly 4-iodophenylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 28782-78-7
N-(tert-butyloxycarbonyl)-(S)-alanylglycine

: 540-37-4
p-aminoiodobenzene

: 1072115-75-3
L-BocAlaGly 4-iodophenylamide

Guidance literature:: N-(tert-butyloxycarbonyl)-(S)-alanylglycine; With benzotriazol-1-ol; 1,2-dichloro-ethane; In chloroform; at 20 ℃; for 0.25h;

p-aminoiodobenzene; In chloroform; at 20 ℃; for 65h;
DOI:10.1002/ejoc.200800433

Reference yield:

: 15761-38-3
L-N-Boc-Ala

: C₈H₉IN₂O*C₂HF₃O₂

: 1072115-75-3
L-BocAlaGly 4-iodophenylamide

Guidance literature:: L-N-Boc-Ala; With triethylamine; isobutyl chloroformate; In chloroform; at 0 ℃; for 0.5h;

C₈H₉IN₂O*C₂HF₃O₂; With triethylamine; In chloroform; at 20 ℃; for 12h;
DOI:10.1021/jacs.6b13171

Reference yield:

: 540-37-4
p-aminoiodobenzene

: 1072115-75-3
L-BocAlaGly 4-iodophenylamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: isobutyl chloroformate; triethylamine / chloroform / 0.5 h / 0 °C

1.2: 12 h / 20 °C

2.1: dichloromethane / 5 h / 20 °C

3.1: isobutyl chloroformate; triethylamine / chloroform / 0.5 h / 0 °C

3.2: 12 h / 20 °C

With triethylamine; isobutyl chloroformate; In dichloromethane; chloroform;
DOI:10.1021/jacs.6b13171