benzyl [(1Z)-{[(2,4-dichlorophenyl)acetyl]amino}(methylthio)methylene]carbamate

Base Information

• Chemical Name: benzyl [(1Z)-{[(2,4-dichlorophenyl)acetyl]amino}(methylthio)methylene]carbamate
• CAS No.: 1142400-41-6
• Molecular Formula: C₁₈H₁₆Cl₂N₂O₃S
• Molecular Weight: 411.309

Synonyms:benzyl [(1Z)-{[(2,4-dichlorophenyl)acetyl]amino}(methylthio)methylene]carbamate

Chemical Property of benzyl [(1Z)-{[(2,4-dichlorophenyl)acetyl]amino}(methylthio)methylene]carbamate

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Technology Process of benzyl [(1Z)-{[(2,4-dichlorophenyl)acetyl]amino}(methylthio)methylene]carbamate

There total 1 articles about benzyl [(1Z)-{[(2,4-dichlorophenyl)acetyl]amino}(methylthio)methylene]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

2,4-dichlorophenylacetic acid (19719-28-9) + (Z)-benzyl amino(methylthio)methylenecarbamate → benzyl [(1Z)-{[(2,4-dichlorophenyl)acetyl]amino}(methylthio)methylene]carbamate (1142400-41-6)

Guidance literature:

With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 23 ℃; for 12h;

DOI:10.1016/j.tetlet.2008.12.042

Reference yield: 70.0%

(4-fluorobenzyl)-hydrazine hydrochloride (1059626-05-9,1000805-93-5) + benzyl [(1Z)-{[(2,4-dichlorophenyl)acetyl]amino}(methylthio)methylene]carbamate (1142400-41-6) → 5-(2,4-dichloro-benzyl)-1-(4-fluoro-benzyl)-1-H-[1,2,4]triazol-3-ylamine (1142400-17-6)

Guidance literature:

With triethylamine; at 160 ℃; for 0.5h; Microwave irradiation;

DOI:10.1016/j.tetlet.2008.12.042

Reference yield: 65.0%

benzyl [(1Z)-{[(2,4-dichlorophenyl)acetyl]amino}(methylthio)methylene]carbamate (1142400-41-6) + (2-hydroxyethyl)hydrazine hydrochloride → C11H12Cl2N4O (1142400-31-4)

Guidance literature:

With triethylamine; at 160 ℃; for 0.5h; Microwave irradiation;

DOI:10.1016/j.tetlet.2008.12.042

upstream raw materials:

2,4-dichlorophenylacetic acid

Downstream raw materials:

5-(2,4-dichloro-benzyl)-1-(4-fluoro-benzyl)-1-H-[1,2,4]triazol-3-ylamine

C₁₄H₁₈Cl₂N₄

C₁₄H₁₆Cl₂N₄O

C₁₁H₁₂Cl₂N₄

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