4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)-1-(2-(trifluoromethyl)-10H-phenothiazin-10-yl)butan-2-ol

Base Information

Chemical Name:4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)-1-(2-(trifluoromethyl)-10H-phenothiazin-10-yl)butan-2-ol
CAS No.:1387627-07-7
Molecular Formula:C₂₅H₂₂F₃N₅O₂S
Molecular Weight:513.543
Hs Code.:

Synonyms:4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)-1-(2-(trifluoromethyl)-10H-phenothiazin-10-yl)butan-2-ol

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Chemical Property of 4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)-1-(2-(trifluoromethyl)-10H-phenothiazin-10-yl)butan-2-ol

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Technology Process of 4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)-1-(2-(trifluoromethyl)-10H-phenothiazin-10-yl)butan-2-ol

There total 3 articles about 4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)-1-(2-(trifluoromethyl)-10H-phenothiazin-10-yl)butan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₂₃BF₃N₅OS

: 1387627-07-7
4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)-1-(2-(trifluoromethyl)-10H-phenothiazin-10-yl)butan-2-ol

Guidance literature:: With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; methanol; water; at 0 - 20 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.bmc.2012.05.065

Reference yield:

: 92-30-8
2-(trifluoromethyl)-10H-phenothiazine

: 1387627-07-7
4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)-1-(2-(trifluoromethyl)-10H-phenothiazin-10-yl)butan-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 48.33 h

2: dimethylsulfide borane complex / tetrahydrofuran / 24 h / 0 - 20 °C / Inert atmosphere

3: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; methanol; water / 24 h / 0 - 20 °C / Inert atmosphere

With dimethylsulfide borane complex; dihydrogen peroxide; sodium hydride; sodium hydroxide; In tetrahydrofuran; methanol; water; mineral oil;
DOI:10.1016/j.bmc.2012.05.065

Reference yield:

: 3-(4-methoxyphenyl)-tetrazolo[1,5-a]pyridin-4-ium tetrafluoroborate

: 1387627-07-7
4-(2-(4-methoxyphenyl)-2H-tetrazol-5-yl)-1-(2-(trifluoromethyl)-10H-phenothiazin-10-yl)butan-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 48.33 h

2: dimethylsulfide borane complex / tetrahydrofuran / 24 h / 0 - 20 °C / Inert atmosphere

3: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; methanol; water / 24 h / 0 - 20 °C / Inert atmosphere

With dimethylsulfide borane complex; dihydrogen peroxide; sodium hydride; sodium hydroxide; In tetrahydrofuran; methanol; water; mineral oil;
DOI:10.1016/j.bmc.2012.05.065