2-amino-3-[5-(benzyloxy)indole-3-yl]-4-methoxybutanoic acid ethyl ester

Base Information

Chemical Name:2-amino-3-[5-(benzyloxy)indole-3-yl]-4-methoxybutanoic acid ethyl ester
CAS No.:169525-70-6
Molecular Formula:C₂₂H₂₆N₂O₄
Molecular Weight:382.459
Hs Code.:

Synonyms:2-amino-3-[5-(benzyloxy)indole-3-yl]-4-methoxybutanoic acid ethyl ester

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Chemical Property of 2-amino-3-[5-(benzyloxy)indole-3-yl]-4-methoxybutanoic acid ethyl ester

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 2-amino-3-[5-(benzyloxy)indole-3-yl]-4-methoxybutanoic acid ethyl ester

There total 4 articles about 2-amino-3-[5-(benzyloxy)indole-3-yl]-4-methoxybutanoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 210160-48-8
3-[5-(benzyloxy)indole-3-yl]-4-methoxy-2-nitrobutanoic acid ethyl ester

: 169525-70-6
2-amino-3-[5-(benzyloxy)indole-3-yl]-4-methoxybutanoic acid ethyl ester

Guidance literature:: With hydrogen; nickel; In ethanol; for 36h;
DOI:10.1021/jm970460b

Reference yield:

: 1215-59-4
5-benzyloxy-1H-indole

: 169525-70-6
2-amino-3-[5-(benzyloxy)indole-3-yl]-4-methoxybutanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / toluene / 4 h / Heating

2: 8.1 g / hydrogen / Raney nickel / ethanol / 6 h / 1900 Torr

With hydrogen; acetic acid; nickel; In ethanol; toluene; 1: Substitution / 2: Catalytic hydrogenation;

Reference yield:

: (E)-4-Methoxy-2-nitro-but-2-enoic acid ethyl ester

: 169525-70-6
2-amino-3-[5-(benzyloxy)indole-3-yl]-4-methoxybutanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / glacial acetic acid / toluene / 1.25 h / Heating

2: 83 percent / H₂ / Raney nickel / ethanol / 36 h

With hydrogen; acetic acid; nickel; In ethanol; toluene;
DOI:10.1021/jm970460b