3-[5-(benzyloxy)indole-3-yl]-4-methoxy-2-nitrobutanoic acid ethyl ester

Base Information

Chemical Name:3-[5-(benzyloxy)indole-3-yl]-4-methoxy-2-nitrobutanoic acid ethyl ester
CAS No.:210160-48-8
Molecular Formula:C₂₂H₂₄N₂O₆
Molecular Weight:412.442
Hs Code.:

Synonyms:3-[5-(benzyloxy)indole-3-yl]-4-methoxy-2-nitrobutanoic acid ethyl ester

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Chemical Property of 3-[5-(benzyloxy)indole-3-yl]-4-methoxy-2-nitrobutanoic acid ethyl ester

Chemical Property:

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Technology Process of 3-[5-(benzyloxy)indole-3-yl]-4-methoxy-2-nitrobutanoic acid ethyl ester

There total 1 articles about 3-[5-(benzyloxy)indole-3-yl]-4-methoxy-2-nitrobutanoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1215-59-4
5-benzyloxy-1H-indole

: 87824-17-7
4-methoxy-3-hydroxy-2-nitrobutyric acid ethyl ester

: 210160-48-8
3-[5-(benzyloxy)indole-3-yl]-4-methoxy-2-nitrobutanoic acid ethyl ester

Guidance literature:: With acetic acid; In toluene; for 4h; Heating;

Reference yield: 83.0%

: 210160-48-8
3-[5-(benzyloxy)indole-3-yl]-4-methoxy-2-nitrobutanoic acid ethyl ester

: 169525-70-6
2-amino-3-[5-(benzyloxy)indole-3-yl]-4-methoxybutanoic acid ethyl ester

Guidance literature:: With hydrogen; nickel; In ethanol; for 36h;
DOI:10.1021/jm970460b

Reference yield:

: 210160-48-8
3-[5-(benzyloxy)indole-3-yl]-4-methoxy-2-nitrobutanoic acid ethyl ester

: 83910-44-5
3-carboethoxy-4-methoxymethyl-6-benzyloxy-β-carboline

Guidance literature:: Multi-step reaction with 2 steps

1.1: 8.1 g / hydrogen / Raney nickel / ethanol / 6 h / 1900 Torr

2.1: ethyl acetate; H₂O / 20 °C

2.2: Pd/C / xylene / Heating

With hydrogen; nickel; In ethanol; water; ethyl acetate; 1.1: Catalytic hydrogenation / 2.1: Condensation / 2.2: Dehydrogenation;