p-Terephthalotoluidide

Base Information

Chemical Name:p-Terephthalotoluidide
CAS No.:36360-33-5
Molecular Formula:C22H20N2O2
Molecular Weight:344.413
Hs Code.:
NSC Number:71193
DSSTox Substance ID:DTXSID30290816
Wikidata:Q82028609
Mol file:36360-33-5.mol

Synonyms:p-Terephthalotoluidide;36360-33-5;NSC71193;n,n'-bis(4-methylphenyl)benzene-1,4-dicarboxamide;Teraphthalo-p-toluidide;Cambridge id 5181408;Oprea1_148735;DTXSID30290816;VVBLWQQCOFKUTA-UHFFFAOYSA-N;NSC-71193;STL260519;AKOS001400472;N,N'-DI-P-TOLYL-TEREPHTHALAMIDE;N,N'-bis(4-methylphenyl)terephthalamide;SR-01000406818;N1,N4-bis(4-methylphenyl)benzene-1,4-dicarboxamide;SR-01000406818-1;Z28134869;5181-40-8

Suppliers and Price of p-Terephthalotoluidide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of p-Terephthalotoluidide

Chemical Property:

XLogP3:4.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:344.152477885
Heavy Atom Count:26
Complexity:425

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)NC(=O)C2=CC=C(C=C2)C(=O)NC3=CC=C(C=C3)C

Technology Process of p-Terephthalotoluidide

There total 2 articles about p-Terephthalotoluidide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106-49-0,12221-03-3
p-toluidine

: 100-20-9
terephthaloyl chloride

: 36360-33-5
Terephthalsaeure-bis-(p-toluidid)

Guidance literature:: With triethylamine; In toluene; at 15 ℃; Rate constant; Thermodynamic data; Kinetics; other temperatures; without triethylamine; ΔS(excit.), ΔE(excit.);

Reference yield:

: 36360-33-5
Terephthalsaeure-bis-(p-toluidid)

Guidance literature:: DOI:10.1021/je60053a006

Reference yield:

: 36360-33-5
Terephthalsaeure-bis-(p-toluidid)

: 17852-28-7
2-amino-5-methylbenzophenone

Guidance literature:: Multi-step reaction with 3 steps

1: PCl₅, SOCl₂ / 4 h / 100 °C

2: 1.) tetrabutylammonium bromide, NaOH, H₂O / 1.) CH₂Cl₂, 20 deg C, 4 h, 2.) toluene, 100 deg C, 6 h

3: 93 percent / HCl, H₂O / 2 h / 100 °C

With hydrogenchloride; sodium hydroxide; thionyl chloride; phosphorus pentachloride; tetrabutylammomium bromide; water;