Methyl uronate, triethylammonium salt

Base Information

Chemical Name:Methyl uronate, triethylammonium salt
CAS No.:136597-49-4
Molecular Formula:C₆H₁₅N*C₄₈H₄₄O₁₉S
Molecular Weight:1058.12
Hs Code.:

Methyl <benzyl 2,3-di-O-benzoyl-4-O-(2,3-di-O-benzoyl-6-O-sulfo-β-D-galactopyranosyl)-β-D-glucopyranosid>uronate, triethylammonium salt

Synonyms:Methyl uronate, triethylammonium salt

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Chemical Property of Methyl uronate, triethylammonium salt

Chemical Property:

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Technology Process of Methyl uronate, triethylammonium salt

There total 12 articles about Methyl uronate, triethylammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18404-72-3
benzyl 4-O-β-D-galactopyranosyl-β-D-glucopyranoside

: 136597-49-4
Methyl uronate, triethylammonium salt

Guidance literature:: Multi-step reaction with 8 steps

1: 66 percent / ZnCl₂ / 48 h

2: 93 percent / imidazole / dimethylformamide / Ambient temperature

3: 85 percent / pyridine / Ambient temperature

4: 95 percent / Bu₄NF / tetrahydrofuran / 0.5 h / Ambient temperature

5: 1) CrO₃, pyridine 2) Ac₂O / 1) CH₂Cl₂, DMF, 10 min, r.t. 2) 18 h, r.t.

6: CF₃CO₂H / CH₂Cl₂ / 10 h / 0 °C

7: tetrahydrofuran; diethyl ether / 0.17 h / Ambient temperature

8: 1) SO₃*Me₃N 2) Et₃N / 1) DMF, 14 d, r.t. 2) toluene

With pyridine; 1H-imidazole; chromium(VI) oxide; trimethyl-sulfo-ammonium betaine; tetrabutyl ammonium fluoride; acetic anhydride; triethylamine; trifluoroacetic acid; zinc(II) chloride; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(91)84026-B

Reference yield:

: 100-52-7
benzaldehyde

: 136597-49-4
Methyl uronate, triethylammonium salt

Guidance literature:: Multi-step reaction with 8 steps

1: 66 percent / ZnCl₂ / 48 h

2: 93 percent / imidazole / dimethylformamide / Ambient temperature

3: 85 percent / pyridine / Ambient temperature

4: 95 percent / Bu₄NF / tetrahydrofuran / 0.5 h / Ambient temperature

5: 1) CrO₃, pyridine 2) Ac₂O / 1) CH₂Cl₂, DMF, 10 min, r.t. 2) 18 h, r.t.

6: CF₃CO₂H / CH₂Cl₂ / 10 h / 0 °C

7: tetrahydrofuran; diethyl ether / 0.17 h / Ambient temperature

8: 1) SO₃*Me₃N 2) Et₃N / 1) DMF, 14 d, r.t. 2) toluene

With pyridine; 1H-imidazole; chromium(VI) oxide; trimethyl-sulfo-ammonium betaine; tetrabutyl ammonium fluoride; acetic anhydride; triethylamine; trifluoroacetic acid; zinc(II) chloride; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(91)84026-B

Reference yield:

: 136235-43-3
Benzyl 4',6'-O-benzylidene-β-lactopyranoside

: 136597-49-4
Methyl uronate, triethylammonium salt

Guidance literature:: Multi-step reaction with 7 steps

1: 93 percent / imidazole / dimethylformamide / Ambient temperature

2: 85 percent / pyridine / Ambient temperature

3: 95 percent / Bu₄NF / tetrahydrofuran / 0.5 h / Ambient temperature

4: 1) CrO₃, pyridine 2) Ac₂O / 1) CH₂Cl₂, DMF, 10 min, r.t. 2) 18 h, r.t.

5: CF₃CO₂H / CH₂Cl₂ / 10 h / 0 °C

6: tetrahydrofuran; diethyl ether / 0.17 h / Ambient temperature

7: 1) SO₃*Me₃N 2) Et₃N / 1) DMF, 14 d, r.t. 2) toluene

With pyridine; 1H-imidazole; chromium(VI) oxide; trimethyl-sulfo-ammonium betaine; tetrabutyl ammonium fluoride; acetic anhydride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(91)84026-B