cyclohexyl 2-acetamido-2-deoxy-1-thio-3,4,6-tri-O-acetyl-α-D-glucopyranoside

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Chemical Name:cyclohexyl 2-acetamido-2-deoxy-1-thio-3,4,6-tri-O-acetyl-α-D-glucopyranoside
CAS No.:479255-65-7
Molecular Formula:C₂₀H₃₁NO₈S
Molecular Weight:445.534
Hs Code.:

Synonyms:cyclohexyl 2-acetamido-2-deoxy-1-thio-3,4,6-tri-O-acetyl-α-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cyclohexyl 2-acetamido-2-deoxy-1-thio-3,4,6-tri-O-acetyl-α-D-glucopyranoside

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Technology Process of cyclohexyl 2-acetamido-2-deoxy-1-thio-3,4,6-tri-O-acetyl-α-D-glucopyranoside

There total 3 articles about cyclohexyl 2-acetamido-2-deoxy-1-thio-3,4,6-tri-O-acetyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 343925-61-1
(2R,3S,4R,5R,6R)-5-acetamido-2-(acetoxymethyl)-6-mercaptotetrahydro-2H-pyran-3,4-diyl diacetate

: 110-83-8
cyclohexene

: 479255-65-7
cyclohexyl 2-acetamido-2-deoxy-1-thio-3,4,6-tri-O-acetyl-α-D-glucopyranoside

Guidance literature:: With 2,2'-azobis(isobutyronitrile); In chloroform; for 3h; Heating;
DOI:10.1021/ol0269796

Reference yield:

: 67145-37-3,67109-74-4
(3aR,5R,6S,7R,7aR)-5-(acetoxymethyl)-6,7-diacetoxy-2-methyl-5,6,7,7a-tetrahydro-3aH-pyrano[3,2-d]thiazole

: 479255-65-7
cyclohexyl 2-acetamido-2-deoxy-1-thio-3,4,6-tri-O-acetyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / trifluoroacetic acid / methanol; H₂O

2: 79 percent / 2,2'-azobis(isobutyronitrile) / CHCl₃ / 3 h / Heating

With 2,2'-azobis(isobutyronitrile); trifluoroacetic acid; In methanol; chloroform; water;
DOI:10.1021/ol0269796

Reference yield:

: 3006-60-8,4539-83-7,6730-10-5,7772-79-4,7784-54-5,10385-50-9,14086-90-9,26151-16-6,76375-60-5,76375-61-6,95341-98-3,95341-99-4,134451-91-5,134451-96-0,136982-81-5,145375-11-7,148347-15-3
2-acetamido-1,3,4,6-tetra-O-acetyl-2-deoxy-β-D-glucopyranose

: 479255-65-7
cyclohexyl 2-acetamido-2-deoxy-1-thio-3,4,6-tri-O-acetyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / Lawesson's reagent / toluene / 1.5 h / 80 °C

2: 100 percent / trifluoroacetic acid / methanol; H₂O

3: 79 percent / 2,2'-azobis(isobutyronitrile) / CHCl₃ / 3 h / Heating

With Lawessons reagent; 2,2'-azobis(isobutyronitrile); trifluoroacetic acid; In methanol; chloroform; water; toluene;
DOI:10.1021/ol0269796