3-(3-{[{2-[(6-hydroxyhexyl)oxy]ethyl}(methyl)amino]methyl}phenyl)imidazolidine-2,4-dione

Base Information

Chemical Name:3-(3-{[{2-[(6-hydroxyhexyl)oxy]ethyl}(methyl)amino]methyl}phenyl)imidazolidine-2,4-dione
CAS No.:956235-80-6
Molecular Formula:C₁₉H₂₉N₃O₄
Molecular Weight:363.457
Hs Code.:

Synonyms:3-(3-{[{2-[(6-hydroxyhexyl)oxy]ethyl}(methyl)amino]methyl}phenyl)imidazolidine-2,4-dione

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Chemical Property of 3-(3-{[{2-[(6-hydroxyhexyl)oxy]ethyl}(methyl)amino]methyl}phenyl)imidazolidine-2,4-dione

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Technology Process of 3-(3-{[{2-[(6-hydroxyhexyl)oxy]ethyl}(methyl)amino]methyl}phenyl)imidazolidine-2,4-dione

There total 10 articles about 3-(3-{[{2-[(6-hydroxyhexyl)oxy]ethyl}(methyl)amino]methyl}phenyl)imidazolidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 956235-79-3
3-(3-{[(2-{[6-(benzyloxy)hexyl]oxy}ethyl)(methyl)amino]methyl}phenyl)imidazolidine-2,4-dione

: 956235-80-6
3-(3-{[{2-[(6-hydroxyhexyl)oxy]ethyl}(methyl)amino]methyl}phenyl)imidazolidine-2,4-dione

Guidance literature:: With hydrogenchloride; hydrogen; palladium 10% on activated carbon; In ethanol; at 20 ℃; for 5h;

Reference yield:

: 943742-18-5
(3-amino-benzyl)-methyl-carbamic acid benzyl ester

: 956235-80-6
3-(3-{[{2-[(6-hydroxyhexyl)oxy]ethyl}(methyl)amino]methyl}phenyl)imidazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 5 steps

1.1: dichloromethane / 1 h / 20 °C

2.1: sodium hydroxide; water / ethanol / 4.5 h / 20 °C

3.1: hydrogenchloride / water / 18 h / 140 °C

3.2: pH 7

4.1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 18 h / 70 °C

5.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / ethanol / 5 h / 20 °C

With hydrogenchloride; sodium hydroxide; water; hydrogen; sodium hydrogencarbonate; palladium 10% on activated carbon; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 943742-17-4
methyl-(3-nitro-benzyl)-carbamic acid benzyl ester

: 956235-80-6
3-(3-{[{2-[(6-hydroxyhexyl)oxy]ethyl}(methyl)amino]methyl}phenyl)imidazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 6 steps

1.1: ethanol; tin(ll) chloride / 2 h / Heating / reflux

2.1: dichloromethane / 1 h / 20 °C

3.1: sodium hydroxide; water / ethanol / 4.5 h / 20 °C

4.1: hydrogenchloride / water / 18 h / 140 °C

4.2: pH 7

5.1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 18 h / 70 °C

6.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / ethanol / 5 h / 20 °C

With hydrogenchloride; sodium hydroxide; ethanol; water; hydrogen; sodium hydrogencarbonate; tin(ll) chloride; palladium 10% on activated carbon; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;