6-{2-[[3-(2,5-dioxoimidazolidin-1-yl)benzyl](methyl)amino]ethoxy}hexyl methanesulfonate

Base Information

Chemical Name:6-{2-[[3-(2,5-dioxoimidazolidin-1-yl)benzyl](methyl)amino]ethoxy}hexyl methanesulfonate
CAS No.:956235-82-8
Molecular Formula:C₂₀H₃₁N₃O₆S
Molecular Weight:441.549
Hs Code.:

Synonyms:6-{2-[[3-(2,5-dioxoimidazolidin-1-yl)benzyl](methyl)amino]ethoxy}hexyl methanesulfonate

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Chemical Property of 6-{2-[[3-(2,5-dioxoimidazolidin-1-yl)benzyl](methyl)amino]ethoxy}hexyl methanesulfonate

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Technology Process of 6-{2-[[3-(2,5-dioxoimidazolidin-1-yl)benzyl](methyl)amino]ethoxy}hexyl methanesulfonate

There total 11 articles about 6-{2-[[3-(2,5-dioxoimidazolidin-1-yl)benzyl](methyl)amino]ethoxy}hexyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.8%

: 956235-80-6
3-(3-{[{2-[(6-hydroxyhexyl)oxy]ethyl}(methyl)amino]methyl}phenyl)imidazolidine-2,4-dione

: 124-63-0
methanesulfonyl chloride

: 956235-82-8
6-{2-[[3-(2,5-dioxoimidazolidin-1-yl)benzyl](methyl)amino]ethoxy}hexyl methanesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 24h;

Reference yield:

: 943742-18-5
(3-amino-benzyl)-methyl-carbamic acid benzyl ester

: 956235-82-8
6-{2-[[3-(2,5-dioxoimidazolidin-1-yl)benzyl](methyl)amino]ethoxy}hexyl methanesulfonate

Guidance literature:: Multi-step reaction with 6 steps

1.1: dichloromethane / 1 h / 20 °C

2.1: sodium hydroxide; water / ethanol / 4.5 h / 20 °C

3.1: hydrogenchloride / water / 18 h / 140 °C

3.2: pH 7

4.1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 18 h / 70 °C

5.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / ethanol / 5 h / 20 °C

6.1: triethylamine / dichloromethane / 24 h / 20 °C

With hydrogenchloride; sodium hydroxide; water; hydrogen; sodium hydrogencarbonate; triethylamine; palladium 10% on activated carbon; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 943742-17-4
methyl-(3-nitro-benzyl)-carbamic acid benzyl ester

: 956235-82-8
6-{2-[[3-(2,5-dioxoimidazolidin-1-yl)benzyl](methyl)amino]ethoxy}hexyl methanesulfonate

Guidance literature:: Multi-step reaction with 7 steps

1.1: ethanol; tin(ll) chloride / 2 h / Heating / reflux

2.1: dichloromethane / 1 h / 20 °C

3.1: sodium hydroxide; water / ethanol / 4.5 h / 20 °C

4.1: hydrogenchloride / water / 18 h / 140 °C

4.2: pH 7

5.1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 18 h / 70 °C

6.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / ethanol / 5 h / 20 °C

7.1: triethylamine / dichloromethane / 24 h / 20 °C

With hydrogenchloride; sodium hydroxide; ethanol; water; hydrogen; sodium hydrogencarbonate; triethylamine; tin(ll) chloride; palladium 10% on activated carbon; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;