4-(4-carboxymethoxycarbonyl-butyl)-2-oxo-hexahydro-thieno[3,4-d]imidazole-1-carboxylic acid 4-(tert-butyl-dimethyl-silanyloxy)-phenyl ester

Base Information

Chemical Name:4-(4-carboxymethoxycarbonyl-butyl)-2-oxo-hexahydro-thieno[3,4-d]imidazole-1-carboxylic acid 4-(tert-butyl-dimethyl-silanyloxy)-phenyl ester
CAS No.:817602-46-3
Molecular Formula:C₂₅H₃₆N₂O₈SSi
Molecular Weight:552.721
Hs Code.:

4-(4-carboxymethoxycarbonyl-butyl)-2-oxo-hexahydro-thieno[3,4-<i>d</i>]imidazole-1-carboxylic acid 4-(<i>tert</i>-butyl-dimethyl-silanyloxy)-phenyl ester

Synonyms:4-(4-carboxymethoxycarbonyl-butyl)-2-oxo-hexahydro-thieno[3,4-d]imidazole-1-carboxylic acid 4-(tert-butyl-dimethyl-silanyloxy)-phenyl ester

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Chemical Property of 4-(4-carboxymethoxycarbonyl-butyl)-2-oxo-hexahydro-thieno[3,4-d]imidazole-1-carboxylic acid 4-(tert-butyl-dimethyl-silanyloxy)-phenyl ester

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Technology Process of 4-(4-carboxymethoxycarbonyl-butyl)-2-oxo-hexahydro-thieno[3,4-d]imidazole-1-carboxylic acid 4-(tert-butyl-dimethyl-silanyloxy)-phenyl ester

There total 5 articles about 4-(4-carboxymethoxycarbonyl-butyl)-2-oxo-hexahydro-thieno[3,4-d]imidazole-1-carboxylic acid 4-(tert-butyl-dimethyl-silanyloxy)-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 817602-45-2
4-(4-tert-butoxycarbonylmethoxycarbonyl-butyl)-2-oxo-hexahydro-thieno[3,4-d]imidazole-1-carboxylic acid 4-(tert-butyl-dimethyl-silanyloxy)-phenyl ester

: 817602-46-3
4-(4-carboxymethoxycarbonyl-butyl)-2-oxo-hexahydro-thieno[3,4-d]imidazole-1-carboxylic acid 4-(tert-butyl-dimethyl-silanyloxy)-phenyl ester

Guidance literature:: With trifluoroacetic acid; In chloroform; at 20 ℃; for 15h;
DOI:10.1021/ja0459330

Reference yield:

: 108534-47-0
4-(tert-butyldimethylsilyloxy)phenol

: 817602-46-3
4-(4-carboxymethoxycarbonyl-butyl)-2-oxo-hexahydro-thieno[3,4-d]imidazole-1-carboxylic acid 4-(tert-butyl-dimethyl-silanyloxy)-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / toluene; diethyl ether / 2 h / 0 °C

2.1: LiHMDS / tetrahydrofuran / 0.08 h / -10 °C

2.2: tetrahydrofuran / 1 h

3.1: 100 percent / trifluoroacetic acid / CHCl₃ / 15 h / 20 °C

With triethylamine; trifluoroacetic acid; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; chloroform; toluene;
DOI:10.1021/ja0459330

Reference yield:

: 58-85-5,22879-79-4
biotin

: 817602-46-3
4-(4-carboxymethoxycarbonyl-butyl)-2-oxo-hexahydro-thieno[3,4-d]imidazole-1-carboxylic acid 4-(tert-butyl-dimethyl-silanyloxy)-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: K₂CO₃ / dimethylsulfoxide / 5 h / 20 °C

2.1: LiHMDS / tetrahydrofuran / 0.08 h / -10 °C

2.2: tetrahydrofuran / 1 h

3.1: 100 percent / trifluoroacetic acid / CHCl₃ / 15 h / 20 °C

With potassium carbonate; trifluoroacetic acid; lithium hexamethyldisilazane; In tetrahydrofuran; chloroform; dimethyl sulfoxide;
DOI:10.1021/ja0459330