benzyl 2,6-di(acetamido)-2,6-dideoxy-3-O--α-D-glucopyranoside

Base Information

Chemical Name:benzyl 2,6-di(acetamido)-2,6-dideoxy-3-O--α-D-glucopyranoside
CAS No.:83055-31-6
Molecular Formula:C₂₁H₃₀N₂O₈
Molecular Weight:438.478
Hs Code.:

benzyl 2,6-di(acetamido)-2,6-dideoxy-3-O-<D-1-(methoxycarbonyl)ethyl>-α-D-glucopyranoside

Synonyms:benzyl 2,6-di(acetamido)-2,6-dideoxy-3-O--α-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 2,6-di(acetamido)-2,6-dideoxy-3-O--α-D-glucopyranoside

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Technology Process of benzyl 2,6-di(acetamido)-2,6-dideoxy-3-O--α-D-glucopyranoside

There total 2 articles about benzyl 2,6-di(acetamido)-2,6-dideoxy-3-O--α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74221-00-4
benzyl 2-acetamido-2-deoxy-6-O-mesyl-3-O--α-D-glucopyranoside

: 83055-31-6
benzyl 2,6-di(acetamido)-2,6-dideoxy-3-O--α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / sodium azide / dimethylformamide / 5 h / 80 °C / Heating

2: 1.) hydrogen / 1.) 10 percent Pd-C / 1.) methanol, room temperature, 40 min; 2.) methanol, room temperature, 30 min

With sodium azide; hydrogen; palladium on activated charcoal; In N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)80688-6

Reference yield:

: 108-24-7
acetic anhydride

: 77268-46-3
benzyl 2-acetamido-6-azido-2,6-dideoxy-3-O--α-D-glucopyranoside

: 83055-31-6
benzyl 2,6-di(acetamido)-2,6-dideoxy-3-O--α-D-glucopyranoside

Guidance literature:: With hydrogen; palladium on activated charcoal; Yield given. Multistep reaction; 1.) methanol, room temperature, 40 min; 2.) methanol, room temperature, 30 min;
DOI:10.1016/S0008-6215(00)80688-6