C₄₅H₆₆O₁₀

Base Information

Chemical Name:C₄₅H₆₆O₁₀
CAS No.:1312441-97-6
Molecular Formula:C₄₅H₆₆O₁₀
Molecular Weight:767.013
Hs Code.:

C<sub>45</sub>H<sub>66</sub>O<sub>10</sub>

Synonyms:C₄₅H₆₆O₁₀

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Chemical Property of C₄₅H₆₆O₁₀

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Technology Process of C₄₅H₆₆O₁₀

There total 18 articles about C₄₅H₆₆O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1312441-99-8
C₄₅H₆₈O₁₀

: 1312441-97-6
C₄₅H₆₆O₁₀

Guidance literature:: With pyridine; Dess-Martin periodane; In dichloromethane; at 25 ℃; for 5h;
DOI:10.1021/ol201426c

Reference yield:

: 1312441-87-4
C₁₁H₂₀O₃

: 1312441-97-6
C₄₅H₆₆O₁₀

Guidance literature:: Multi-step reaction with 13 steps

1.1: triethylamine; (-)-diisopinocamphenylborane chloride / diethyl ether / 1 h / 0 °C

1.2: 18 h / -78 - -20 °C

2.1: tetramethylammonium triacetoxyborohydride / acetic acid; acetonitrile / 4 h / -20 - 25 °C

3.1: pyridinium p-toluenesulfonate / dichloromethane / 2 h / 0 - 25 °C

4.1: diisobutylaluminium hydride / toluene / 1 h / -20 °C

5.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 25 °C

6.1: pyridinium p-toluenesulfonate / methanol; chloroform / 48 h / 25 °C

7.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C

7.2: 6 h / 25 °C

8.1: tert.-butyl lithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; pentane / 0.08 h / -78 °C

8.2: 1 h / -78 °C

9.1: manganese(IV) oxide / dichloromethane / 8 h / 25 °C

10.1: 4-toluenesulfonyl azide; potassium carbonate / acetonitrile / 2 h / 25 °C

10.2: 18 h / 25 °C

11.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

11.2: 0.5 h / -78 - 25 °C

11.3: 3 h / Reflux

12.1: hydrogen / ethanol / 40 h / 50 °C

13.1: pyridine; Dess-Martin periodane / dichloromethane / 5 h / 25 °C

With pyridine; manganese(IV) oxide; 4-toluenesulfonyl azide; hydrogen; tert.-butyl lithium; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; potassium carbonate; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; (-)-diisopinocamphenylborane chloride; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; ethanol; dichloromethane; chloroform; acetic acid; toluene; acetonitrile; mineral oil; pentane; 1.2: Aldol condensation / 11.3: Suzuki coupling / 13.1: Dess-Martin oxidation;
DOI:10.1021/ol201426c

Reference yield:

: 1312441-90-9
C₂₉H₄₆O₆

: 1312441-97-6
C₄₅H₆₆O₁₀

Guidance literature:: Multi-step reaction with 12 steps

1.1: tetramethylammonium triacetoxyborohydride / acetic acid; acetonitrile / 4 h / -20 - 25 °C

2.1: pyridinium p-toluenesulfonate / dichloromethane / 2 h / 0 - 25 °C

3.1: diisobutylaluminium hydride / toluene / 1 h / -20 °C

4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 25 °C

5.1: pyridinium p-toluenesulfonate / methanol; chloroform / 48 h / 25 °C

6.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C

6.2: 6 h / 25 °C

7.1: tert.-butyl lithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; pentane / 0.08 h / -78 °C

7.2: 1 h / -78 °C

8.1: manganese(IV) oxide / dichloromethane / 8 h / 25 °C

9.1: 4-toluenesulfonyl azide; potassium carbonate / acetonitrile / 2 h / 25 °C

9.2: 18 h / 25 °C

10.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

10.2: 0.5 h / -78 - 25 °C

10.3: 3 h / Reflux

11.1: hydrogen / ethanol / 40 h / 50 °C

12.1: pyridine; Dess-Martin periodane / dichloromethane / 5 h / 25 °C

With pyridine; manganese(IV) oxide; 4-toluenesulfonyl azide; hydrogen; tert.-butyl lithium; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; potassium carbonate; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; dichloromethane; chloroform; acetic acid; toluene; acetonitrile; mineral oil; pentane; 10.3: Suzuki coupling / 12.1: Dess-Martin oxidation;
DOI:10.1021/ol201426c