iodomethyl 4-(5-(cyclopropylcarbamoyl)-2-methylphenylamino)-5-methylpyrrolo[1,2-f][1,2,4]triazine-6-carbonyl(propyl)carbamate

Base Information

Chemical Name:iodomethyl 4-(5-(cyclopropylcarbamoyl)-2-methylphenylamino)-5-methylpyrrolo[1,2-f][1,2,4]triazine-6-carbonyl(propyl)carbamate
CAS No.:948842-84-0
Molecular Formula:C₂₄H₂₇IN₆O₄
Molecular Weight:590.421
Hs Code.:

Synonyms:iodomethyl 4-(5-(cyclopropylcarbamoyl)-2-methylphenylamino)-5-methylpyrrolo[1,2-f][1,2,4]triazine-6-carbonyl(propyl)carbamate

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Chemical Property of iodomethyl 4-(5-(cyclopropylcarbamoyl)-2-methylphenylamino)-5-methylpyrrolo[1,2-f][1,2,4]triazine-6-carbonyl(propyl)carbamate

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Technology Process of iodomethyl 4-(5-(cyclopropylcarbamoyl)-2-methylphenylamino)-5-methylpyrrolo[1,2-f][1,2,4]triazine-6-carbonyl(propyl)carbamate

There total 4 articles about iodomethyl 4-(5-(cyclopropylcarbamoyl)-2-methylphenylamino)-5-methylpyrrolo[1,2-f][1,2,4]triazine-6-carbonyl(propyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 623152-17-0
BMS-582949

: 948842-84-0
iodomethyl 4-(5-(cyclopropylcarbamoyl)-2-methylphenylamino)-5-methylpyrrolo[1,2-f][1,2,4]triazine-6-carbonyl(propyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap / N,N-dimethyl-formamide / 60 °C

2.1: lithium hexamethyldisilazane / tetrahydrofuran / -45 °C

2.2: -45 - 20 °C

3.1: sodium iodide / acetone / Reflux

With dmap; sodium iodide; lithium hexamethyldisilazane; In tetrahydrofuran; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.bmcl.2013.03.022

Reference yield:

: 948842-83-9
C₂₉H₃₅ClN₆O₆

: 948842-84-0
iodomethyl 4-(5-(cyclopropylcarbamoyl)-2-methylphenylamino)-5-methylpyrrolo[1,2-f][1,2,4]triazine-6-carbonyl(propyl)carbamate

Guidance literature:: With sodium iodide; In acetone; Reflux;
DOI:10.1016/j.bmcl.2013.03.022

Reference yield:

: 948842-81-7
C₂₇H₃₄N₆O₄

: 948842-84-0
iodomethyl 4-(5-(cyclopropylcarbamoyl)-2-methylphenylamino)-5-methylpyrrolo[1,2-f][1,2,4]triazine-6-carbonyl(propyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / -45 °C

1.2: -45 - 20 °C

2.1: sodium iodide / acetone / Reflux

With sodium iodide; lithium hexamethyldisilazane; In tetrahydrofuran; acetone;
DOI:10.1016/j.bmcl.2013.03.022