N-{2-[4-(biphenyl-2-ylcarbamoyloxy)piperidin-1-yl]ethyl}-N-methylisophthalamic acid

Base Information

• Chemical Name: N-{2-[4-(biphenyl-2-ylcarbamoyloxy)piperidin-1-yl]ethyl}-N-methylisophthalamic acid
• CAS No.: 909899-76-9
• Molecular Formula: C₂₉H₃₁N₃O₅
• Molecular Weight: 501.582

Synonyms:N-{2-[4-(biphenyl-2-ylcarbamoyloxy)piperidin-1-yl]ethyl}-N-methylisophthalamic acid

Chemical Property of N-{2-[4-(biphenyl-2-ylcarbamoyloxy)piperidin-1-yl]ethyl}-N-methylisophthalamic acid

Chemical Property:

Purity/Quality:

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Technology Process of N-{2-[4-(biphenyl-2-ylcarbamoyloxy)piperidin-1-yl]ethyl}-N-methylisophthalamic acid

There total 2 articles about N-{2-[4-(biphenyl-2-ylcarbamoyloxy)piperidin-1-yl]ethyl}-N-methylisophthalamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(2-{[(3-Formylphenyl)carbonyl](methyl)amino}ethyl)piperidin-4-yl biphenyl-2-ylcarbamate (909899-75-8) → N-{2-[4-(biphenyl-2-ylcarbamoyloxy)piperidin-1-yl]ethyl}-N-methylisophthalamic acid (909899-76-9)

Guidance literature:

With sodium chloroformate; aminosulfonic acid; In water; acetic acid; at 0 - 20 ℃; for 1.667h;

Reference yield:

biphenyl-2-ylcarbamic acid 1-(2-{[3-(2-tert-butoxycarbonylaminoethylcarbamoyl)-benzoyl]methylamino}ethyl)piperidin-4-yl ester (909899-74-7) → N-{2-[4-(biphenyl-2-ylcarbamoyloxy)piperidin-1-yl]ethyl}-N-methylisophthalamic acid (909899-76-9)

Guidance literature:

With sodium chlorite; aminosulfonic acid; acetic acid; In water; at 0 - 20 ℃; for 1.66667h;

Reference yield:

N-{2-[4-(biphenyl-2-ylcarbamoyloxy)piperidin-1-yl]ethyl}-N-methylisophthalamic acid (909899-76-9) + N-BOC-1,2-diaminoethane (57260-73-8) → biphenyl-2-ylcarbamic acid 1-(2-{[3-(2-tert-butoxycarbonylaminoethylcarbamoyl)-benzoyl]methylamino}ethyl)piperidin-4-yl ester (909899-74-7)

Guidance literature:

Product distribution / selectivity;

upstream raw materials:

1-(2-{[(3-Formylphenyl)carbonyl](methyl)amino}ethyl)piperidin-4-yl biphenyl-2-ylcarbamate

biphenyl-2-ylcarbamic acid 1-(2-{[3-(2-tert-butoxycarbonylaminoethylcarbamoyl)-benzoyl]methylamino}ethyl)piperidin-4-yl ester

Downstream raw materials:

biphenyl-2-ylcarbamic acid 1-(2-{[3-(2-tert-butoxycarbonylaminoethylcarbamoyl)-benzoyl]methylamino}ethyl)piperidin-4-yl ester

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