2,3-bisbenzyloxy-N-[1,3-bis-(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl]-terephthalic acid monoamide-(4-nitrophenyl) ester

Base Information

• Chemical Name: 2,3-bisbenzyloxy-N-[1,3-bis-(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl]-terephthalic acid monoamide-(4-nitrophenyl) ester
• CAS No.: 872462-89-0
• Molecular Formula: C₆₅H₆₄N₂O₁₃
• Molecular Weight: 1081.23

Synonyms:2,3-bisbenzyloxy-N-[1,3-bis-(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl]-terephthalic acid monoamide-(4-nitrophenyl) ester

Chemical Property of 2,3-bisbenzyloxy-N-[1,3-bis-(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl]-terephthalic acid monoamide-(4-nitrophenyl) ester

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Technology Process of 2,3-bisbenzyloxy-N-[1,3-bis-(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl]-terephthalic acid monoamide-(4-nitrophenyl) ester

There total 1 articles about 2,3-bisbenzyloxy-N-[1,3-bis-(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl]-terephthalic acid monoamide-(4-nitrophenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + 2,3-bis(benzyloxy)-N-(1,3-bis(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl)-terephthalic acid monoamide (872462-88-9) → 2,3-bisbenzyloxy-N-[1,3-bis-(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl]-terephthalic acid monoamide-(4-nitrophenyl) ester (872462-89-0)

Guidance literature:

With dicyclohexyl-carbodiimide; In tetrahydrofuran; at 20 ℃; for 20h;

Reference yield: 94.0%

2,3-bisbenzyloxy-N-[1,3-bis-(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl]-terephthalic acid monoamide-(4-nitrophenyl) ester (872462-89-0) + 4-(amino)-5-[bis-(2-{3-benzyloxy-1-[1,3-bis-(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl]-6-methyl-2-oxo-1,2-dihydropyridine-4-carbonyl}-aminoethyl)amino]-pentane carboxylic acid → C171H189N7O30

Guidance literature:

In dichloromethane; at 20 ℃; for 72h;

upstream raw materials:

4-nitro-phenol

2,3-bis(benzyloxy)-N-(1,3-bis(2-benzyloxy-1-benzyloxymethyl-ethoxy)-prop-2-yl)-terephthalic acid monoamide

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