4-[1-oxo-3-(2-hydroxy-3-quinolinyl)-2-propenyl]-3-(4-methoxyphenyl)sydnone

Base Information

Chemical Name:4-[1-oxo-3-(2-hydroxy-3-quinolinyl)-2-propenyl]-3-(4-methoxyphenyl)sydnone
CAS No.:1335106-48-3
Molecular Formula:C₂₁H₁₅N₃O₅
Molecular Weight:389.367
Hs Code.:

Synonyms:4-[1-oxo-3-(2-hydroxy-3-quinolinyl)-2-propenyl]-3-(4-methoxyphenyl)sydnone

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Chemical Property of 4-[1-oxo-3-(2-hydroxy-3-quinolinyl)-2-propenyl]-3-(4-methoxyphenyl)sydnone

Chemical Property:

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Technology Process of 4-[1-oxo-3-(2-hydroxy-3-quinolinyl)-2-propenyl]-3-(4-methoxyphenyl)sydnone

There total 2 articles about 4-[1-oxo-3-(2-hydroxy-3-quinolinyl)-2-propenyl]-3-(4-methoxyphenyl)sydnone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 34356-36-0
4-acetyl-3-(4-methoxyphenyl)sydnone

: 91301-03-0
2-hydroxyquinoline-3-carboxaldehyde

: 1335106-48-3
4-[1-oxo-3-(2-hydroxy-3-quinolinyl)-2-propenyl]-3-(4-methoxyphenyl)sydnone

Guidance literature:: With hydrogenchloride; In ethanol; water; at 5 - 20 ℃;

Reference yield:

: 3815-80-3
3-(p-anisyl)sydnone

: 1335106-48-3
4-[1-oxo-3-(2-hydroxy-3-quinolinyl)-2-propenyl]-3-(4-methoxyphenyl)sydnone

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus pentoxide / benzene / 5.17 h / Reflux

2: hydrogenchloride / ethanol; water / 5 - 20 °C

With hydrogenchloride; phosphorus pentoxide; In ethanol; water; benzene; 2: Claisen Schmidt condensation;