1-(2,3-dimethoxyphenyl)-5-(4-bromophenyl)-5-oxopentan-2-yl O-ethyl carbonodithioate

Base Information

Chemical Name:1-(2,3-dimethoxyphenyl)-5-(4-bromophenyl)-5-oxopentan-2-yl O-ethyl carbonodithioate
CAS No.:1309875-69-1
Molecular Formula:C₂₂H₂₅BrO₄S₂
Molecular Weight:497.474
Hs Code.:

Synonyms:1-(2,3-dimethoxyphenyl)-5-(4-bromophenyl)-5-oxopentan-2-yl O-ethyl carbonodithioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2,3-dimethoxyphenyl)-5-(4-bromophenyl)-5-oxopentan-2-yl O-ethyl carbonodithioate

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Technology Process of 1-(2,3-dimethoxyphenyl)-5-(4-bromophenyl)-5-oxopentan-2-yl O-ethyl carbonodithioate

There total 1 articles about 1-(2,3-dimethoxyphenyl)-5-(4-bromophenyl)-5-oxopentan-2-yl O-ethyl carbonodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1861-48-9
dithiocarbonic acid S-[2-(4-bromo-phenyl)-2-oxo-ethyl] ester O-ethyl ester

: 19754-21-3
1-allyl-2,3-dimethoxy-benzene

: 1309875-69-1
1-(2,3-dimethoxyphenyl)-5-(4-bromophenyl)-5-oxopentan-2-yl O-ethyl carbonodithioate

Guidance literature:: With dilauryl peroxide; In ethyl acetate; Reflux; Inert atmosphere;
DOI:10.1021/ol2012204

Reference yield: 50.0%

: 1309875-69-1
1-(2,3-dimethoxyphenyl)-5-(4-bromophenyl)-5-oxopentan-2-yl O-ethyl carbonodithioate

: 1309875-77-1
4-(2,3-dimethoxybenzyl)-6-bromo-3,4-dihydronaphthalen-1(2H)-one

Guidance literature:: With dilauryl peroxide; In ethyl acetate; Reflux; Inert atmosphere;
DOI:10.1021/ol2012204

Reference yield:

: 1309875-69-1
1-(2,3-dimethoxyphenyl)-5-(4-bromophenyl)-5-oxopentan-2-yl O-ethyl carbonodithioate

: C₂₁H₂₂BrNO₄

Guidance literature:: Multi-step reaction with 3 steps

1: dilauryl peroxide / ethyl acetate / Reflux; Inert atmosphere

2: hydroxylamine hydrochloride; sodium acetate / ethanol / Reflux; Inert atmosphere

3: 0.67 h / 80 °C / Inert atmosphere

With dilauryl peroxide; hydroxylamine hydrochloride; sodium acetate; In ethanol; ethyl acetate;
DOI:10.1021/ol2012204