2-(3-chloromethyl-2-hydroxy-5-tert-butylbenzyl)-6-chloromethyl-4-tert-butylphenol

Base Information

• Chemical Name: 2-(3-chloromethyl-2-hydroxy-5-tert-butylbenzyl)-6-chloromethyl-4-tert-butylphenol
• CAS No.: 182946-02-7
• Molecular Formula: C₂₃H₃₀Cl₂O₂
• Molecular Weight: 409.396

Synonyms:2-(3-chloromethyl-2-hydroxy-5-tert-butylbenzyl)-6-chloromethyl-4-tert-butylphenol

Chemical Property of 2-(3-chloromethyl-2-hydroxy-5-tert-butylbenzyl)-6-chloromethyl-4-tert-butylphenol

Chemical Property:

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Technology Process of 2-(3-chloromethyl-2-hydroxy-5-tert-butylbenzyl)-6-chloromethyl-4-tert-butylphenol

There total 2 articles about 2-(3-chloromethyl-2-hydroxy-5-tert-butylbenzyl)-6-chloromethyl-4-tert-butylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

bis(5-tert-butyl-2-hydroxy-3-hydroxymethyl-phenyl)methane (2467-07-4) → 2-(3-chloromethyl-2-hydroxy-5-tert-butylbenzyl)-6-chloromethyl-4-tert-butylphenol (182946-02-7)

Guidance literature:

With thionyl chloride; In benzene; at 20 ℃; for 5h;

DOI:10.1002/jhet.5570370113

Reference yield:

para-tert-butylphenol (98-54-4) → 2-(3-chloromethyl-2-hydroxy-5-tert-butylbenzyl)-6-chloromethyl-4-tert-butylphenol (182946-02-7)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous NaOH

2: HCl

With hydrogenchloride; sodium hydroxide;

DOI:10.1007/BF00899467

Reference yield: 22.0%

2-(3-chloromethyl-2-hydroxy-5-tert-butylbenzyl)-6-chloromethyl-4-tert-butylphenol (182946-02-7) + L-tyrosine methyl ester HCl (3417-91-2) → 3,17-bis[(1S)-2-(4-hydroxyphenyl)-1-(methoxycarbonyl)ethyl]-7,13,21,27-tetra-tert-butyl-29,30,31,32-tetrahydroxy-2,3,16,17-tetrahomo-3,17-diazapentacyclo[23.3.1.15,9.111,15.119,23]dotriaconta-1(28),5,7,9(29),11,13,15(30),19,21,23(31),25,27-dodecen

Guidance literature:

With sodium carbonate; In N,N-dimethyl-formamide; at 30 ℃; for 4h;

DOI:10.1002/jhet.5570370113

upstream raw materials:

bis(5-tert-butyl-2-hydroxy-3-hydroxymethyl-phenyl)methane

para-tert-butylphenol

Downstream raw materials:

2-<3-<3-(5-tert-Butylsalicyl)-5-tert-butylsalicyl>-5-tert-butylsalicyl>-4-tert-butylphenol

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