p-tolyl 6-azido-2,3,4-tri-O-benzoyl-6-deoxy-1-thio-α-D-mannopyranoside

Base Information

Chemical Name:p-tolyl 6-azido-2,3,4-tri-O-benzoyl-6-deoxy-1-thio-α-D-mannopyranoside
CAS No.:1473360-07-4
Molecular Formula:C₃₄H₂₉N₃O₇S
Molecular Weight:623.686
Hs Code.:

Synonyms:p-tolyl 6-azido-2,3,4-tri-O-benzoyl-6-deoxy-1-thio-α-D-mannopyranoside

Suppliers and Price of p-tolyl 6-azido-2,3,4-tri-O-benzoyl-6-deoxy-1-thio-α-D-mannopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of p-tolyl 6-azido-2,3,4-tri-O-benzoyl-6-deoxy-1-thio-α-D-mannopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of p-tolyl 6-azido-2,3,4-tri-O-benzoyl-6-deoxy-1-thio-α-D-mannopyranoside

There total 5 articles about p-tolyl 6-azido-2,3,4-tri-O-benzoyl-6-deoxy-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₃H₁₇N₃O₄S

: 98-88-4
benzoyl chloride

: 1473360-07-4
p-tolyl 6-azido-2,3,4-tri-O-benzoyl-6-deoxy-1-thio-α-D-mannopyranoside

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 2h; pH=9;
DOI:10.1016/j.carres.2013.08.010

Reference yield:

: 210170-40-4
1,2,3,4-tetra-O-acetyl-6-azido-6-deoxy-α-D-mannopyranoside

: 1473360-07-4
p-tolyl 6-azido-2,3,4-tri-O-benzoyl-6-deoxy-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: boron trifluoride diethyl etherate / dichloromethane / 12 h / 20 °C

2: methanol; sodium methylate / 0.5 h / pH 9

3: triethylamine; dmap / dichloromethane / 2 h / 20 °C / pH 9

With methanol; dmap; boron trifluoride diethyl etherate; sodium methylate; triethylamine; In dichloromethane;
DOI:10.1016/j.carres.2013.08.010

Reference yield:

: 1473360-05-2
p-tolyl 6-azido-2,3,4-tri-O-acetyl-6-deoxy-1-thio-α-D-mannopyranoside

: 1473360-07-4
p-tolyl 6-azido-2,3,4-tri-O-benzoyl-6-deoxy-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; sodium methylate / 0.5 h / pH 9

2: triethylamine; dmap / dichloromethane / 2 h / 20 °C / pH 9

With methanol; dmap; sodium methylate; triethylamine; In dichloromethane;
DOI:10.1016/j.carres.2013.08.010