1-(6-benzyloxymethyl-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)-3-[((2,6-dichloro-4-methoxyphenyl)-(2,4,6-trichlorophenyl)methoxy)methyl]-1H-pyrimidine-2,4-dione

Base Information

Chemical Name:1-(6-benzyloxymethyl-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)-3-[((2,6-dichloro-4-methoxyphenyl)-(2,4,6-trichlorophenyl)methoxy)methyl]-1H-pyrimidine-2,4-dione
CAS No.:1380572-76-8
Molecular Formula:C₃₄H₃₁Cl₅N₂O₈
Molecular Weight:772.894
Hs Code.:

1-(6-benzyloxymethyl-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)-3-[((2,6-dichloro-4-methoxyphenyl)-(2,4,6-trichlorophenyl)methoxy)methyl]-1H-pyrimidine-2,4-dione

Synonyms:1-(6-benzyloxymethyl-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)-3-[((2,6-dichloro-4-methoxyphenyl)-(2,4,6-trichlorophenyl)methoxy)methyl]-1H-pyrimidine-2,4-dione

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Chemical Property of 1-(6-benzyloxymethyl-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)-3-[((2,6-dichloro-4-methoxyphenyl)-(2,4,6-trichlorophenyl)methoxy)methyl]-1H-pyrimidine-2,4-dione

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Technology Process of 1-(6-benzyloxymethyl-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)-3-[((2,6-dichloro-4-methoxyphenyl)-(2,4,6-trichlorophenyl)methoxy)methyl]-1H-pyrimidine-2,4-dione

There total 1 articles about 1-(6-benzyloxymethyl-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)-3-[((2,6-dichloro-4-methoxyphenyl)-(2,4,6-trichlorophenyl)methoxy)methyl]-1H-pyrimidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1380572-75-7
C₂₇H₂₅Cl₅N₂O₈

: 100-39-0
benzyl bromide

: 1380572-76-8
1-(6-benzyloxymethyl-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)-3-[((2,6-dichloro-4-methoxyphenyl)-(2,4,6-trichlorophenyl)methoxy)methyl]-1H-pyrimidine-2,4-dione

Guidance literature:: C₂₇H₂₅Cl₅N₂O₈; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.0833333h;

benzyl bromide; In N,N-dimethyl-formamide; 1,1,2,2-tetrachloroethane; for 3h;
DOI:10.1016/j.tet.2012.03.121

Reference yield:

: 1380572-76-8
1-(6-benzyloxymethyl-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl)-3-[((2,6-dichloro-4-methoxyphenyl)-(2,4,6-trichlorophenyl)methoxy)methyl]-1H-pyrimidine-2,4-dione

: 1380572-75-7
C₂₇H₂₅Cl₅N₂O₈

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In water; isopropyl alcohol; for 2h; chemoselective reaction;
DOI:10.1016/j.tet.2012.03.121