C₂₅H₃₃N₅O₅S

Base Information

Chemical Name:C₂₅H₃₃N₅O₅S
CAS No.:1374962-07-8
Molecular Formula:C₂₅H₃₃N₅O₅S
Molecular Weight:515.634
Hs Code.:

C<sub>25</sub>H<sub>33</sub>N<sub>5</sub>O<sub>5</sub>S

Synonyms:C₂₅H₃₃N₅O₅S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₃₃N₅O₅S

Chemical Property:

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Technology Process of C₂₅H₃₃N₅O₅S

There total 5 articles about C₂₅H₃₃N₅O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.7%

: 1374962-75-0
N-benzenesulfonyl-D,L-leucyl-L-proline-[(4-cyanophenyl)methyl]amide

: 1374962-07-8
C₂₅H₃₃N₅O₅S

Guidance literature:: With hydroxylamine hydrochloride; sodium carbonate; In ethanol; water; for 2h; Inert atmosphere; Reflux;

Reference yield:

: 328-39-2,21675-61-6,25248-98-0,70-45-1
LEUCINE

: 1374962-07-8
C₂₅H₃₃N₅O₅S

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide / 1,4-dioxane / 4 h / 0 - 20 °C / pH 9 - 10

2: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 4 h / 20 °C / Inert atmosphere; Cooling

3: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 20 °C

4: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 5.33 h / 0 - 20 °C / Inert atmosphere

5: hydroxylamine hydrochloride; sodium carbonate / water; ethanol / 2 h / Inert atmosphere; Reflux

With palladium 10% on activated carbon; hydroxylamine hydrochloride; hydrogen; sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In 1,4-dioxane; methanol; ethanol; dichloromethane; water;

Reference yield:

: 1374962-73-8
N-benzenesulfonyl-D,L-leucyl-L-proline benzyl ester

: 1374962-07-8
C₂₅H₃₃N₅O₅S

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 20 °C

2: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 5.33 h / 0 - 20 °C / Inert atmosphere

3: hydroxylamine hydrochloride; sodium carbonate / water; ethanol / 2 h / Inert atmosphere; Reflux

With palladium 10% on activated carbon; hydroxylamine hydrochloride; hydrogen; sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In methanol; ethanol; dichloromethane; water;