benzoic acid 3-(diethylamino)-2-hydroxy-3-oxopropyl ester

Base Information

• Chemical Name: benzoic acid 3-(diethylamino)-2-hydroxy-3-oxopropyl ester
• CAS No.: 855526-48-6
• Molecular Formula: C₁₄H₁₉NO₄
• Molecular Weight: 265.309

Synonyms:benzoic acid 3-(diethylamino)-2-hydroxy-3-oxopropyl ester

Chemical Property of benzoic acid 3-(diethylamino)-2-hydroxy-3-oxopropyl ester

Chemical Property:

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Technology Process of benzoic acid 3-(diethylamino)-2-hydroxy-3-oxopropyl ester

There total 2 articles about benzoic acid 3-(diethylamino)-2-hydroxy-3-oxopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

benzoic acid anhydride (93-97-0) + N,N-diethyl-2,3-dihydroxypropanamide (477211-58-8) → benzoic acid 3-(diethylamino)-2-hydroxy-3-oxopropyl ester (855526-48-6)

Guidance literature:

In benzene; at 20 ℃; for 36h;

DOI:10.1021/jo050246s

Reference yield:

N,N-diethyl-2,2-dimethyl-1,3-dioxolane-4-carboxamide (855526-45-3) → benzoic acid 3-(diethylamino)-2-hydroxy-3-oxopropyl ester (855526-48-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / acetic acid / H₂O / 1 h / Heating

2: 35 percent / benzene / 36 h / 20 °C

With acetic acid; In water; benzene;

DOI:10.1021/jo050246s

Reference yield: 70.0%

benzoic acid 3-(diethylamino)-2-hydroxy-3-oxopropyl ester (855526-48-6) → benzoic acid 3-(diethylamino)-2,3-dioxopropyl ester (855526-50-0)

Guidance literature:

With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1021/jo050246s

upstream raw materials:

benzoic acid anhydride

N,N-diethyl-2,3-dihydroxypropanamide

N,N-diethyl-2,2-dimethyl-1,3-dioxolane-4-carboxamide

Downstream raw materials:

benzoic acid 3-(diethylamino)-2,3-dioxopropyl ester

3-ethyl-2-methyl-5-methylene-oxazolidin-4-one

3-ethyl-5-hydroxy-2,5-dimethyl-oxazolidin-4-one

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