C₄₇H₆₃NO₁₅

Base Information

Chemical Name:C₄₇H₆₃NO₁₅
CAS No.:176039-75-1
Molecular Formula:C₄₇H₆₃NO₁₅
Molecular Weight:882.015
Hs Code.:

C<sub>47</sub>H<sub>63</sub>NO<sub>15</sub>

Synonyms:C₄₇H₆₃NO₁₅

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Chemical Property of C₄₇H₆₃NO₁₅

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Technology Process of C₄₇H₆₃NO₁₅

There total 7 articles about C₄₇H₆₃NO₁₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: C₅₅H₇₁NO₁₆

: 176039-75-1
C₄₇H₆₃NO₁₅

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; for 1h; Ambient temperature;
DOI:10.1016/0040-4020(96)00035-X

Reference yield:

: 51-67-2
tyrosamine

: 176039-75-1
C₄₇H₆₃NO₁₅

Guidance literature:: Multi-step reaction with 5 steps

1: 626 mg / aq. NaOH / ethanol / 39 h / Ambient temperature

2: 66 percent / NIS, TfOH, molecular sieves 4 Angstroem / 1,2-dichloro-ethane; diethyl ether / 0.25 h / 0 °C

3: 89 percent / potassium tert-butoxide / methanol / 3 h / Ambient temperature

4: 89 percent / NIS, TfOH, molecular sieves 4 Angstroem / 1,2-dichloro-ethane; diethyl ether / 0.25 h / -30 °C

5: 67 percent / DDQ / CH₂Cl₂; H₂O / 1 h / Ambient temperature

With sodium hydroxide; N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; potassium tert-butylate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In methanol; diethyl ether; ethanol; dichloromethane; water; 1,2-dichloro-ethane;
DOI:10.1016/0040-4020(96)00035-X

Reference yield:

: 146399-58-8
ethyl 3-O-acetyl-2,4-di-O-methyl-1-thio-α-L-rhamnopyranoside

: 176039-75-1
C₄₇H₆₃NO₁₅

Guidance literature:: Multi-step reaction with 4 steps

1: 66 percent / NIS, TfOH, molecular sieves 4 Angstroem / 1,2-dichloro-ethane; diethyl ether / 0.25 h / 0 °C

2: 89 percent / potassium tert-butoxide / methanol / 3 h / Ambient temperature

3: 89 percent / NIS, TfOH, molecular sieves 4 Angstroem / 1,2-dichloro-ethane; diethyl ether / 0.25 h / -30 °C

4: 67 percent / DDQ / CH₂Cl₂; H₂O / 1 h / Ambient temperature

With N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; potassium tert-butylate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In methanol; diethyl ether; dichloromethane; water; 1,2-dichloro-ethane;
DOI:10.1016/0040-4020(96)00035-X