C₁₈H₂₂O₅

Base Information

• Chemical Name: C₁₈H₂₂O₅
• CAS No.: 1429339-09-2
• Molecular Formula: C₁₈H₂₂O₅
• Molecular Weight: 318.37
• Mol file: 1429339-09-2.mol

Synonyms:C₁₈H₂₂O₅

Chemical Property of C₁₈H₂₂O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₈H₂₂O₅

There total 2 articles about C₁₈H₂₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,5-bis(benzaldehydeoxy)-3-oxopentane (82645-24-7) → C18H22O5 (1429339-09-2)

Guidance literature:

With sodium tetrahydroborate;

DOI:10.1039/c4ra02174f

Reference yield:

salicylaldehyde (90-02-8) → C18H22O5 (1429339-09-2)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile

2: sodium tetrahydroborate / ethanol

With sodium tetrahydroborate; potassium carbonate; In ethanol; acetonitrile;

DOI:10.1021/ic4030475

Reference yield: 82.0%

C18H22O5 (1429339-09-2) + allyl bromide (106-95-6) → C24H30O5 (1429339-68-3)

Guidance literature:

With sodium hydride; In tetrahydrofuran; at 20 ℃; for 20h;

DOI:10.1016/j.tet.2015.06.070

upstream raw materials:

1,5-bis(benzaldehydeoxy)-3-oxopentane

salicylaldehyde

Downstream raw materials:

C₂₄H₂₆O₅

C₁₈H₂₀Cl₂O₃

C₂₄H₃₀O₅

Refernces

• 1、 Naveen,Babu, Srinivasarao Arulananda. "Ring-closing metathesis reaction-based synthesis of new classes of polyether macrocyclic systems". supporting information. p. 7758 - 7781. Retrieved 2015/09/08.
• 2、 Ryu, Hyunsoo,Park, Ki-Min,Ikeda, Mari,Habata, Yoichi,Lee, Shim Sung. "A ditopic O4S2 macrocycle and its hard, soft, and hard/soft metal complexes exhibiting endo-, exo-, or endo/exocyclic coordination: Synthesis, crystal structures, NMR titration, and physical properties". . p. 4029 - 4038. Retrieved 2014/05/06.