4-(3-(2,3-dichlorobenzyl)-2-methyl-7-nitro-3H-benzo[d]imidazol-5-yl)morpholine

Base Information

Chemical Name:4-(3-(2,3-dichlorobenzyl)-2-methyl-7-nitro-3H-benzo[d]imidazol-5-yl)morpholine
CAS No.:1372539-85-9
Molecular Formula:C₁₉H₁₈Cl₂N₄O₃
Molecular Weight:421.283
Hs Code.:

Synonyms:4-(3-(2,3-dichlorobenzyl)-2-methyl-7-nitro-3H-benzo[d]imidazol-5-yl)morpholine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(3-(2,3-dichlorobenzyl)-2-methyl-7-nitro-3H-benzo[d]imidazol-5-yl)morpholine

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Technology Process of 4-(3-(2,3-dichlorobenzyl)-2-methyl-7-nitro-3H-benzo[d]imidazol-5-yl)morpholine

There total 5 articles about 4-(3-(2,3-dichlorobenzyl)-2-methyl-7-nitro-3H-benzo[d]imidazol-5-yl)morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 110-91-8,99108-56-2
morpholine

: 1372539-84-8
6-bromo-1-(2,3-dichlorobenzyl)-2-methyl-4-nitro-1H-benzo[d]imidazole

: 1372539-85-9
4-(3-(2,3-dichlorobenzyl)-2-methyl-7-nitro-3H-benzo[d]imidazol-5-yl)morpholine

Guidance literature:: With caesium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos; In 1,4-dioxane; at 80 ℃; for 3h; Inert atmosphere;

Reference yield:

: 606-22-4
2,6-dinitroaniline

: 1372539-85-9
4-(3-(2,3-dichlorobenzyl)-2-methyl-7-nitro-3H-benzo[d]imidazol-5-yl)morpholine

Guidance literature:: Multi-step reaction with 5 steps

1: bromine / acetic acid / 2 h / 120 °C

2: diammonium sulfide / ethanol / 2 h / 90 °C

3: ethanol; water / 3 h / Reflux

4: potassium carbonate / N,N-dimethyl-formamide / 3 h / 80 °C

5: caesium carbonate / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos / 1,4-dioxane / 3 h / 80 °C / Inert atmosphere

With diammonium sulfide; bromine; potassium carbonate; caesium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos; In 1,4-dioxane; ethanol; water; acetic acid; N,N-dimethyl-formamide;

Reference yield:

: 84752-20-5
4-bromo-6-nitro-1,2-phenylenediamine

: 1372539-85-9
4-(3-(2,3-dichlorobenzyl)-2-methyl-7-nitro-3H-benzo[d]imidazol-5-yl)morpholine

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol; water / 3 h / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 3 h / 80 °C

3: caesium carbonate / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos / 1,4-dioxane / 3 h / 80 °C / Inert atmosphere

With potassium carbonate; caesium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos; In 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide;