5-[2-benzyloxy-4-(1,1-dimethylheptyl)phenyl]-4-carbomethoxy-1,3-cyclohexanedione

Base Information

• Chemical Name: 5-[2-benzyloxy-4-(1,1-dimethylheptyl)phenyl]-4-carbomethoxy-1,3-cyclohexanedione
• CAS No.: 70435-52-8
• Molecular Formula: C₃₀H₃₈O₅
• Molecular Weight: 478.629

Synonyms:5-[2-benzyloxy-4-(1,1-dimethylheptyl)phenyl]-4-carbomethoxy-1,3-cyclohexanedione

Chemical Property of 5-[2-benzyloxy-4-(1,1-dimethylheptyl)phenyl]-4-carbomethoxy-1,3-cyclohexanedione

Chemical Property:

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Technology Process of 5-[2-benzyloxy-4-(1,1-dimethylheptyl)phenyl]-4-carbomethoxy-1,3-cyclohexanedione

There total 4 articles about 5-[2-benzyloxy-4-(1,1-dimethylheptyl)phenyl]-4-carbomethoxy-1,3-cyclohexanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

petroleum ether-ether + trans-4-[2-Benzyloxy-4-(1,1-dimethylheptyl)-phenyl]-3-buten-2-one (70577-12-7) + malonic acid dimethyl ester (108-59-8) → 5-[2-benzyloxy-4-(1,1-dimethylheptyl)phenyl]-4-carbomethoxy-1,3-cyclohexanedione (70435-52-8)

Guidance literature:

With sodium methylate; In methanol;

Reference yield:

1-bromo-2-benzyloxy-4-(1,1-dimethylheptyl)benzene (70120-16-0) → 5-[2-benzyloxy-4-(1,1-dimethylheptyl)phenyl]-4-carbomethoxy-1,3-cyclohexanedione (70435-52-8)

Guidance literature:

Multi-step reaction with 3 steps

1: (i) Mg, (ii) /BRN= 605365/

3: (i) NaOMe, (ii) /BRN= 2674784/

Reference yield:

2-benzyloxy-4-(1,1-dimethylheptyl)benzaldehyde (70436-09-8) → 5-[2-benzyloxy-4-(1,1-dimethylheptyl)phenyl]-4-carbomethoxy-1,3-cyclohexanedione (70435-52-8)

Guidance literature:

Multi-step reaction with 2 steps

2: (i) NaOMe, (ii) /BRN= 2674784/

upstream raw materials:

trans-4-[2-Benzyloxy-4-(1,1-dimethylheptyl)-phenyl]-3-buten-2-one

malonic acid dimethyl ester

1-bromo-2-benzyloxy-4-(1,1-dimethylheptyl)benzene

2-benzyloxy-4-(1,1-dimethylheptyl)benzaldehyde

Downstream raw materials:

5-[2-benzyloxy-4-(1,1-dimethylheptyl)phenyl]-1,3-cyclohexanedione

5-[2-benzyloxy-4-(1,1-dimethylheptyl)phenyl]-2-cyclohexen-1-one

5-[2-Benzyloxy-4-(1,1-dimethylheptyl)phenyl]-3-methyl-2-cyclohexen-1-one

5-[2-Benzyloxy-4-(1,1-dimethyl-heptyl)-phenyl]-3-ethyl-cyclohex-2-enone

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