bis(2,4,6-triisopropylphenyl)-2,7-di-tert-butylfluorenylidenestannane

Base Information

• Chemical Name: bis(2,4,6-triisopropylphenyl)-2,7-di-tert-butylfluorenylidenestannane
• CAS No.: 1137081-03-8
• Molecular Formula: C₅₁H₇₀Sn
• Molecular Weight: 801.827

Synonyms:bis(2,4,6-triisopropylphenyl)-2,7-di-tert-butylfluorenylidenestannane

Chemical Property of bis(2,4,6-triisopropylphenyl)-2,7-di-tert-butylfluorenylidenestannane

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of bis(2,4,6-triisopropylphenyl)-2,7-di-tert-butylfluorenylidenestannane

There total 2 articles about bis(2,4,6-triisopropylphenyl)-2,7-di-tert-butylfluorenylidenestannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,7-di-tert-butyl-9H-fluorene (58775-05-6) → bis(2,4,6-triisopropylphenyl)-2,7-di-tert-butylfluorenylidenestannane (1137081-03-8)

Guidance literature:

Multi-step reaction with 2 steps

1: n-butyllithium / hexane; tetrahydrofuran

2: tert-butyllithium / diethyl ether; pentane

With n-butyllithium; tert-butyllithium; In tetrahydrofuran; diethyl ether; hexane; pentane;

DOI:10.1002/ejic.200701277

Reference yield:

bis(2,4,6-triisopropylphenyl)difluorostannane (142799-36-8) → bis(2,4,6-triisopropylphenyl)-2,7-di-tert-butylfluorenylidenestannane (1137081-03-8)

Guidance literature:

Multi-step reaction with 2 steps

1: n-butyllithium / hexane; tetrahydrofuran

2: tert-butyllithium / diethyl ether; pentane

With n-butyllithium; tert-butyllithium; In tetrahydrofuran; diethyl ether; hexane; pentane;

DOI:10.1002/ejic.200701277

Reference yield: 82.0%

bis(2,4,6-triisopropylphenyl)-2,7-di-tert-butylfluorenylidenestannane (1137081-03-8) + methyl 2-(benzylideneamino)acetate (66646-88-6) → C61H81NO2Sn

Guidance literature:

In diethyl ether; pentane; at -78 - 20 ℃; Inert atmosphere;

DOI:10.1021/om3004916

upstream raw materials:

2,7-di-tert-butyl-9H-fluorene

bis(2,4,6-triisopropylphenyl)difluorostannane

Downstream raw materials:

C₅₈H₇₅NOSn

C₅₈H₇₅NSSn

C₆₅H₈₀OSn

C₆₂H₈₅NOSn

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