C₅₁H₆₀N₂O₁₃

Base Information

Chemical Name:C₅₁H₆₀N₂O₁₃
CAS No.:1255790-57-8
Molecular Formula:C₅₁H₆₀N₂O₁₃
Molecular Weight:909.043
Hs Code.:

C<sub>51</sub>H<sub>60</sub>N<sub>2</sub>O<sub>13</sub>

Synonyms:C₅₁H₆₀N₂O₁₃

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Chemical Property of C₅₁H₆₀N₂O₁₃

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Technology Process of C₅₁H₆₀N₂O₁₃

There total 13 articles about C₅₁H₆₀N₂O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1255790-54-5
10'-((2''S,3''S,4''S,6''S)-3''-acetoxy-4''-benzyloxycarbonylamino-2'',4''-dimethyltetrahydro-2H-pyran-6''-yl)-8'-((2R,4R,5S,6R)-5-benzyloxy-4-dimethylamino-6-methyltetrahydro-2H-pyran-2-yl)-1'-((E)-but-2'''-3n-2'''-yl)-7',12'-dimethoxy-5'-methyl-4'-oxo-4H-naphtho[2,3-h]chromen-11'-yl acetate

: 1255790-57-8
C₅₁H₆₀N₂O₁₃

Guidance literature:: With boron tribromide; In dichloromethane; at -90 ℃;
DOI:10.1021/ja107926f

Reference yield:

: 1255790-48-7
(E)-1''-(5'-((2R,4R,5S,6R)-5-benzyloxy-4-dimethylamino-6-methyltetrahydro-2H-pyran-2-yl)-9',10'-dimethoxy-1'-methoxymethoxy-3'-methyl-8'-(triisopropylsilyloxy)anthracen-2'-yl)-4''-methylhex-4''-en-2''-yn-1''-one

: 1255790-57-8
C₅₁H₆₀N₂O₁₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: ethanol / 3 h / 20 °C / Inert atmosphere

2.1: lithium tetrafluoroborate; water / acetonitrile / 0.25 h / 82 °C / Inert atmosphere; Microwave irradiation

3.1: calcium sulfate; scandium tris(trifluoromethanesulfonate) / 1,2-dichloro-ethane / 67.5 h / -30 - 0 °C / Inert atmosphere

4.1: pyridine; dmap / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

5.1: boron tribromide / dichloromethane / 0.08 h / -90 °C / Inert atmosphere

5.2: -90 - 20 °C / Inert atmosphere

With pyridine; dmap; calcium sulfate; lithium tetrafluoroborate; water; boron tribromide; scandium tris(trifluoromethanesulfonate); In ethanol; dichloromethane; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1016/j.tet.2011.05.117

Reference yield:

: 1273031-50-7
(2R,4R,5S,6R)-5-benzyloxy-2-(6-benzyloxy-5,10-dimethoxy-8-methyl-4-(triisopropylsilyloxy)anthracen-1-yl)-N,N,6-trimethyltetrahydro-2H-pyran-4-amine

: 1255790-57-8
C₅₁H₆₀N₂O₁₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: pyridine; 20% palladium hydroxide on carbon; hydrogen / methanol; ethyl acetate / 2 h

2.1: N-Bromosuccinimide / dichloromethane / 4 h / -78 - 20 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.42 h / 0 - 20 °C / Inert atmosphere

4.1: tert.-butyl lithium / tetrahydrofuran; pentane / 0 h / -78 °C / Inert atmosphere

4.2: -78 - 20 °C / Inert atmosphere

4.3: 20 °C / Inert atmosphere

5.1: barium manganate / benzene / 3.5 h / 20 °C / Inert atmosphere

6.1: ethanol / 3 h / 20 °C / Inert atmosphere

7.1: lithium tetrafluoroborate; water / acetonitrile / 0.25 h / 82 °C / Inert atmosphere; Microwave irradiation

8.1: calcium sulfate; scandium tris(trifluoromethanesulfonate) / 1,2-dichloro-ethane / 67.5 h / -30 - 0 °C / Inert atmosphere

9.1: pyridine; dmap / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

10.1: boron tribromide / dichloromethane / 0.08 h / -90 °C / Inert atmosphere

10.2: -90 - 20 °C / Inert atmosphere

With pyridine; dmap; calcium sulfate; N-Bromosuccinimide; lithium tetrafluoroborate; barium manganate; 20% palladium hydroxide on carbon; water; hydrogen; tert.-butyl lithium; boron tribromide; sodium hydride; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; methanol; ethanol; dichloromethane; ethyl acetate; 1,2-dichloro-ethane; acetonitrile; mineral oil; pentane; benzene;
DOI:10.1016/j.tet.2011.05.117