2,4-dimethylpentan-3-yl 3-(3,4-dimethoxyphenyl)-2-methyl-3-oxopropanoate

Base Information

Chemical Name:2,4-dimethylpentan-3-yl 3-(3,4-dimethoxyphenyl)-2-methyl-3-oxopropanoate
CAS No.:1281895-13-3
Molecular Formula:C₁₉H₂₈O₅
Molecular Weight:336.428
Hs Code.:

Synonyms:2,4-dimethylpentan-3-yl 3-(3,4-dimethoxyphenyl)-2-methyl-3-oxopropanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,4-dimethylpentan-3-yl 3-(3,4-dimethoxyphenyl)-2-methyl-3-oxopropanoate

Chemical Property:

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Technology Process of 2,4-dimethylpentan-3-yl 3-(3,4-dimethoxyphenyl)-2-methyl-3-oxopropanoate

There total 3 articles about 2,4-dimethylpentan-3-yl 3-(3,4-dimethoxyphenyl)-2-methyl-3-oxopropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1061631-12-6
2,4-dimethylpentan-3-yl 3-(3,4-dimethoxyphenyl)-3-oxopropanoate

: 74-88-4
methyl iodide

: 1281895-13-3
2,4-dimethylpentan-3-yl 3-(3,4-dimethoxyphenyl)-2-methyl-3-oxopropanoate

Guidance literature:: With potassium carbonate; In acetone; at 40 ℃; for 24h;
DOI:10.1021/ol400136y

Reference yield:

: 1131-62-0
1-(3,4-dimethoxyphenyl)ethanone

: 1281895-13-3
2,4-dimethylpentan-3-yl 3-(3,4-dimethoxyphenyl)-2-methyl-3-oxopropanoate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 5 h / Reflux

2: zinc(II) oxide / toluene / 24 h / Reflux

3: potassium carbonate / acetone / 24 h / 40 °C

With sodium hydride; potassium carbonate; zinc(II) oxide; In tetrahydrofuran; acetone; toluene; mineral oil;
DOI:10.1021/ol400136y

Reference yield:

: 74053-93-3
methyl 3-(3,4-dimethoxyphenyl)-3-oxopropionate

: 1281895-13-3
2,4-dimethylpentan-3-yl 3-(3,4-dimethoxyphenyl)-2-methyl-3-oxopropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: zinc(II) oxide / toluene / 24 h / Reflux

2: potassium carbonate / acetone / 24 h / 40 °C

With potassium carbonate; zinc(II) oxide; In acetone; toluene;
DOI:10.1021/ol400136y