N-methyl-7-(p-(naphthalen-1-yl(phenyl)amino)phenyl)phenolthiazine-3-carbaldehyde

Base Information

Chemical Name:N-methyl-7-(p-(naphthalen-1-yl(phenyl)amino)phenyl)phenolthiazine-3-carbaldehyde
CAS No.:1361587-74-7
Molecular Formula:C₃₆H₂₆N₂OS
Molecular Weight:534.681
Hs Code.:

Synonyms:N-methyl-7-(p-(naphthalen-1-yl(phenyl)amino)phenyl)phenolthiazine-3-carbaldehyde

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Chemical Property of N-methyl-7-(p-(naphthalen-1-yl(phenyl)amino)phenyl)phenolthiazine-3-carbaldehyde

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Technology Process of N-methyl-7-(p-(naphthalen-1-yl(phenyl)amino)phenyl)phenolthiazine-3-carbaldehyde

There total 4 articles about N-methyl-7-(p-(naphthalen-1-yl(phenyl)amino)phenyl)phenolthiazine-3-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1122570-35-7
p-(tributylstannyl)-N-(phenyl)-N-(naphthalen-1-yl)phenylamine

: 98349-79-2
7-bromo-10-methyl-10H-phenothiazin-3-carbaldehyde

: 1361587-74-7
N-methyl-7-(p-(naphthalen-1-yl(phenyl)amino)phenyl)phenolthiazine-3-carbaldehyde

Guidance literature:: With trans-bis(triphenylphosphine)palladium dichloride; In N,N-dimethyl-formamide; at 90 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c2jm13961h

Reference yield:

: 92-84-2
10H-phenothiazine

: 1361587-74-7
N-methyl-7-(p-(naphthalen-1-yl(phenyl)amino)phenyl)phenolthiazine-3-carbaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0.33 h / Inert atmosphere; Cooling with ice

1.2: Inert atmosphere

2.1: N-Bromosuccinimide / dichloromethane / 8 h / 0 - 20 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / Inert atmosphere

3.2: 6 h / Inert atmosphere

4.1: trans-bis(triphenylphosphine)palladium dichloride / N,N-dimethyl-formamide / 12 h / 90 °C / Inert atmosphere

With N-Bromosuccinimide; n-butyllithium; trans-bis(triphenylphosphine)palladium dichloride; potassium tert-butylate; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2jm13961h

Reference yield:

: 1207-72-3
N-methylphenothiazine

: 1361587-74-7
N-methyl-7-(p-(naphthalen-1-yl(phenyl)amino)phenyl)phenolthiazine-3-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide / dichloromethane / 8 h / 0 - 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / Inert atmosphere

2.2: 6 h / Inert atmosphere

3.1: trans-bis(triphenylphosphine)palladium dichloride / N,N-dimethyl-formamide / 12 h / 90 °C / Inert atmosphere

With N-Bromosuccinimide; n-butyllithium; trans-bis(triphenylphosphine)palladium dichloride; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2jm13961h