C₆₅H₇₃NO₆S

Base Information

Chemical Name:C₆₅H₇₃NO₆S
CAS No.:946073-24-1
Molecular Formula:C₆₅H₇₃NO₆S
Molecular Weight:996.364
Hs Code.:

C<sub>65</sub>H<sub>73</sub>NO<sub>6</sub>S

Synonyms:C₆₅H₇₃NO₆S

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Chemical Property of C₆₅H₇₃NO₆S

Chemical Property:

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Technology Process of C₆₅H₇₃NO₆S

There total 9 articles about C₆₅H₇₃NO₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 946073-45-6
C₅₇H₆₇NO₅

: 69746-43-6
1-iodo-4-thioacetylbenzene

: 946073-24-1
C₆₅H₇₃NO₆S

Guidance literature:: With copper(l) iodide; triethylamine; triphenylphosphine; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In tetrahydrofuran; chloroform; at 20 ℃; for 48h;
DOI:10.1016/j.tet.2007.05.006

Reference yield:

: 153033-31-9
1,4-bis(hexyloxy)-2,5-diiodobenzene

: 946073-24-1
C₆₅H₇₃NO₆S

Guidance literature:: Multi-step reaction with 8 steps

1.1: PPh₃; pyridine; triethylamine / CuI; Pd₂(dba)3 / CHCl₃ / 0.17 h

1.2: 50 percent / CHCl₃ / 48 h / 75 °C

2.1: 96 percent / PPh₃; triethylamine; CuI / Pd₂(dba)3 / CHCl₃ / 48 h / 75 °C

3.1: 79 percent / NaOH / toluene / 24 h / Heating

4.1: 67 percent / PPh₃; triethylamine; CuI / Pd₂(dba)3 / CHCl₃ / 48 h / 75 °C

5.1: 96 percent / TBAF / tetrahydrofuran / 20 °C

6.1: 41 percent / PPh₃; triethylamine; CuI / Pd₂(dba)3 / CHCl₃ / 48 h / 70 °C

7.1: 90 percent / TBAF / tetrahydrofuran / 20 °C

8.1: 60 percent / PPh₃; triethylamine; CuI / Pd₂(dba)3 / CHCl₃; tetrahydrofuran / 48 h / 20 °C

With pyridine; sodium hydroxide; copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine; triphenylphosphine; copper(l) iodide; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In tetrahydrofuran; chloroform; toluene; 2.1: Sonogashira coupling / 4.1: Sonogashira coupling / 6.1: Sonogashira coupling / 8.1: Sonogashira coupling;
DOI:10.1016/j.tet.2007.05.006

Reference yield:

: 872173-78-9
1,4-dihexyloxy-2-(3-hydroxy-3-methylbutynyl)-5-iodobenzene

: 946073-24-1
C₆₅H₇₃NO₆S

Guidance literature:: Multi-step reaction with 7 steps

1: 96 percent / PPh₃; triethylamine; CuI / Pd₂(dba)3 / CHCl₃ / 48 h / 75 °C

2: 79 percent / NaOH / toluene / 24 h / Heating

3: 67 percent / PPh₃; triethylamine; CuI / Pd₂(dba)3 / CHCl₃ / 48 h / 75 °C

4: 96 percent / TBAF / tetrahydrofuran / 20 °C

5: 41 percent / PPh₃; triethylamine; CuI / Pd₂(dba)3 / CHCl₃ / 48 h / 70 °C

6: 90 percent / TBAF / tetrahydrofuran / 20 °C

7: 60 percent / PPh₃; triethylamine; CuI / Pd₂(dba)3 / CHCl₃; tetrahydrofuran / 48 h / 20 °C

With sodium hydroxide; copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine; triphenylphosphine; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In tetrahydrofuran; chloroform; toluene; 1: Sonogashira coupling / 3: Sonogashira coupling / 5: Sonogashira coupling / 7: Sonogashira coupling;
DOI:10.1016/j.tet.2007.05.006