N-{(1S,2E)-4-(benzyloxy)-1-[(1S,2E)-3-iodo-1-methylprop-2-en-1-yl]-2-methylbut-2-en-1-yl}-7-hydroxy-N-methylheptanamide

Base Information

Chemical Name:N-{(1S,2E)-4-(benzyloxy)-1-[(1S,2E)-3-iodo-1-methylprop-2-en-1-yl]-2-methylbut-2-en-1-yl}-7-hydroxy-N-methylheptanamide
CAS No.:1072091-37-2
Molecular Formula:C₂₄H₃₆INO₃
Molecular Weight:513.459
Hs Code.:

Synonyms:N-{(1S,2E)-4-(benzyloxy)-1-[(1S,2E)-3-iodo-1-methylprop-2-en-1-yl]-2-methylbut-2-en-1-yl}-7-hydroxy-N-methylheptanamide

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Chemical Property of N-{(1S,2E)-4-(benzyloxy)-1-[(1S,2E)-3-iodo-1-methylprop-2-en-1-yl]-2-methylbut-2-en-1-yl}-7-hydroxy-N-methylheptanamide

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Technology Process of N-{(1S,2E)-4-(benzyloxy)-1-[(1S,2E)-3-iodo-1-methylprop-2-en-1-yl]-2-methylbut-2-en-1-yl}-7-hydroxy-N-methylheptanamide

There total 15 articles about N-{(1S,2E)-4-(benzyloxy)-1-[(1S,2E)-3-iodo-1-methylprop-2-en-1-yl]-2-methylbut-2-en-1-yl}-7-hydroxy-N-methylheptanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1072091-79-2
C₃₀H₅₀INO₃Si

: 1072091-37-2
N-{(1S,2E)-4-(benzyloxy)-1-[(1S,2E)-3-iodo-1-methylprop-2-en-1-yl]-2-methylbut-2-en-1-yl}-7-hydroxy-N-methylheptanamide

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 19.5h;

Reference yield:

: 1072091-12-3
(2R,3S,4E)-6-(benzyloxy)-3-[(4-methoxyphenyl)amino]-2,4-dimethylhex-4-en-1-ol

: 1072091-37-2
N-{(1S,2E)-4-(benzyloxy)-1-[(1S,2E)-3-iodo-1-methylprop-2-en-1-yl]-2-methylbut-2-en-1-yl}-7-hydroxy-N-methylheptanamide

Guidance literature:: Multi-step reaction with 9 steps

1.1: sulfuric acid; periodic acid / water; acetonitrile / 1.5 h / 20 °C

1.2: 8 h / 20 °C

2.1: Dess-Martin periodane / dichloromethane / 0.17 h / 20 °C

3.1: chromium dichloride / tetrahydrofuran / 5.5 h / 0 - 20 °C

4.1: hydrogenchloride / ethyl acetate / 1 h / 20 °C

5.1: triethylamine / dichloromethane / 3 h / 20 °C

6.1: potassium carbonate / N,N-dimethyl-formamide / 68 h / 20 °C

7.1: lithium hydroxide; mercaptoacetic acid / N,N-dimethyl-formamide / 2.5 h / 20 °C

8.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; diisopropylamine / N,N-dimethyl-formamide / 24 h / 20 °C

9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 19.5 h / 20 °C

With chromium dichloride; hydrogenchloride; lithium hydroxide; sulfuric acid; tetrabutyl ammonium fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; potassium carbonate; Dess-Martin periodane; mercaptoacetic acid; periodic acid; triethylamine; diisopropylamine; In tetrahydrofuran; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1072091-14-5
tert-butyl {(1S,2E)-4-(benzyloxy)-1-[(1R)-2-hydroxy-1-methylethyl]-2-methylbut-2-en-1-yl}carbamate

: 1072091-37-2
N-{(1S,2E)-4-(benzyloxy)-1-[(1S,2E)-3-iodo-1-methylprop-2-en-1-yl]-2-methylbut-2-en-1-yl}-7-hydroxy-N-methylheptanamide

Guidance literature:: Multi-step reaction with 8 steps

1: Dess-Martin periodane / dichloromethane / 0.17 h / 20 °C

2: chromium dichloride / tetrahydrofuran / 5.5 h / 0 - 20 °C

3: hydrogenchloride / ethyl acetate / 1 h / 20 °C

4: triethylamine / dichloromethane / 3 h / 20 °C

5: potassium carbonate / N,N-dimethyl-formamide / 68 h / 20 °C

6: lithium hydroxide; mercaptoacetic acid / N,N-dimethyl-formamide / 2.5 h / 20 °C

7: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; diisopropylamine / N,N-dimethyl-formamide / 24 h / 20 °C

8: tetrabutyl ammonium fluoride / tetrahydrofuran / 19.5 h / 20 °C

With chromium dichloride; hydrogenchloride; lithium hydroxide; tetrabutyl ammonium fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; potassium carbonate; Dess-Martin periodane; mercaptoacetic acid; triethylamine; diisopropylamine; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;