3,7-diacetyl-8-methyl-1,9-diphenyl-4,6-dithia-1,2,9-triazaspiro[4.4]nona-2,7-diene

Base Information

Chemical Name:3,7-diacetyl-8-methyl-1,9-diphenyl-4,6-dithia-1,2,9-triazaspiro[4.4]nona-2,7-diene
CAS No.:543693-98-7
Molecular Formula:C₂₁H₁₉N₃O₂S₂
Molecular Weight:409.533
Hs Code.:

Synonyms:3,7-diacetyl-8-methyl-1,9-diphenyl-4,6-dithia-1,2,9-triazaspiro[4.4]nona-2,7-diene

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Chemical Property of 3,7-diacetyl-8-methyl-1,9-diphenyl-4,6-dithia-1,2,9-triazaspiro[4.4]nona-2,7-diene

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Technology Process of 3,7-diacetyl-8-methyl-1,9-diphenyl-4,6-dithia-1,2,9-triazaspiro[4.4]nona-2,7-diene

There total 4 articles about 3,7-diacetyl-8-methyl-1,9-diphenyl-4,6-dithia-1,2,9-triazaspiro[4.4]nona-2,7-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: C₉H₈N₂O

: 156139-61-6
1-(2,3-dihydro-4-methyl-3-phenyl-2-thioxothiazol-5-yl)-1-ethanone

: 543693-98-7
3,7-diacetyl-8-methyl-1,9-diphenyl-4,6-dithia-1,2,9-triazaspiro[4.4]nona-2,7-diene

Guidance literature:: With triethylamine; In dichloromethane; isopropyl alcohol; at 20 ℃;
DOI:10.1134/S1070428007100193

Reference yield: 50.0%

: 18440-58-9,1017827-91-6
1-(N-phenylhydrazono)-1-chloropropanone

: 156139-61-6
1-(2,3-dihydro-4-methyl-3-phenyl-2-thioxothiazol-5-yl)-1-ethanone

: 543693-98-7
3,7-diacetyl-8-methyl-1,9-diphenyl-4,6-dithia-1,2,9-triazaspiro[4.4]nona-2,7-diene

Guidance literature:: With triethylamine; Reflux;
DOI:10.3390/molecules24091654

Reference yield:

: 1694-29-7
3-chloropentane-2,4-dione

: 543693-98-7
3,7-diacetyl-8-methyl-1,9-diphenyl-4,6-dithia-1,2,9-triazaspiro[4.4]nona-2,7-diene

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 6 h / 20 °C

2: triethylamine / Reflux

With triethylamine; In ethanol;
DOI:10.3390/molecules24091654