(n-butyl)[(2S)-2-hydroxy-2-(p-methoxyphenyl)-ethyl](methyl)sulfonium iodide

Base Information

Chemical Name:(n-butyl)[(2S)-2-hydroxy-2-(p-methoxyphenyl)-ethyl](methyl)sulfonium iodide
CAS No.:1190369-18-6
Molecular Formula:C₁₄H₂₃O₂S*I
Molecular Weight:382.306
Hs Code.:

Synonyms:(n-butyl)[(2S)-2-hydroxy-2-(p-methoxyphenyl)-ethyl](methyl)sulfonium iodide

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Chemical Property of (n-butyl)[(2S)-2-hydroxy-2-(p-methoxyphenyl)-ethyl](methyl)sulfonium iodide

Chemical Property:

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Technology Process of (n-butyl)[(2S)-2-hydroxy-2-(p-methoxyphenyl)-ethyl](methyl)sulfonium iodide

There total 2 articles about (n-butyl)[(2S)-2-hydroxy-2-(p-methoxyphenyl)-ethyl](methyl)sulfonium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1190369-16-4
(-)-(S)-2-(n-butylthio)-1-(p-methoxyphenyl)-ethanol

: 74-88-4
methyl iodide

: 1190369-18-6
(n-butyl)[(2S)-2-hydroxy-2-(p-methoxyphenyl)-ethyl](methyl)sulfonium iodide

Guidance literature:: at 25 ℃; for 24h;
DOI:10.1080/00397910902765578

Reference yield:

: 763-95-1
(S)-(+)-methyl n-butyl sulfoxide

: 1190369-18-6
(n-butyl)[(2S)-2-hydroxy-2-(p-methoxyphenyl)-ethyl](methyl)sulfonium iodide

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / diethyl ether; hexane / 0.17 h / -78 °C / Inert atmosphere

1.2: 0.08 h / -78 - 0 °C / Inert atmosphere

2.1: sodium hydrogensulfite / methanol; water / 4 h / 100 °C / Saturated solution

3.1: 24 h / 25 °C

With n-butyllithium; sodium hydrogensulfite; In methanol; diethyl ether; hexane; water;
DOI:10.1080/00397910902765578

Reference yield:

: 1190369-18-6
(n-butyl)[(2S)-2-hydroxy-2-(p-methoxyphenyl)-ethyl](methyl)sulfonium iodide

: 628-29-5
n-butyl methyl sulfide

: (S)-2-(4-methoxyphenyl)oxirane

Guidance literature:: With dimsylsodium; In tetrahydrofuran; dimethyl sulfoxide; at -10 - 25 ℃; for 1.33333h; Inert atmosphere;
DOI:10.1080/00397910902765578