dimethyl (6E,8E)-9-(3,5-dimethoxyphenyl)-2-oxonona-6,8-dienylphosphonate

Base Information

Chemical Name:dimethyl (6E,8E)-9-(3,5-dimethoxyphenyl)-2-oxonona-6,8-dienylphosphonate
CAS No.:1108750-53-3
Molecular Formula:C₁₉H₂₇O₆P
Molecular Weight:382.394
Hs Code.:

Synonyms:dimethyl (6E,8E)-9-(3,5-dimethoxyphenyl)-2-oxonona-6,8-dienylphosphonate

Suppliers and Price of dimethyl (6E,8E)-9-(3,5-dimethoxyphenyl)-2-oxonona-6,8-dienylphosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of dimethyl (6E,8E)-9-(3,5-dimethoxyphenyl)-2-oxonona-6,8-dienylphosphonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of dimethyl (6E,8E)-9-(3,5-dimethoxyphenyl)-2-oxonona-6,8-dienylphosphonate

There total 2 articles about dimethyl (6E,8E)-9-(3,5-dimethoxyphenyl)-2-oxonona-6,8-dienylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: methyl 8-(3,5-dimethoxyphenyl)octa-5,7-dienoate

: 756-79-6
dimethyl methane phosphonate

: 1108750-53-3
dimethyl (6E,8E)-9-(3,5-dimethoxyphenyl)-2-oxonona-6,8-dienylphosphonate

Guidance literature:: dimethyl methane phosphonate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

methyl 8-(3,5-dimethoxyphenyl)octa-5,7-dienoate; In tetrahydrofuran; hexane; at -78 ℃; Inert atmosphere;
DOI:10.1021/ol101141a

Reference yield: 61.0%

: C₁₉H₂₉O₆P

: 1108750-53-3
dimethyl (6E,8E)-9-(3,5-dimethoxyphenyl)-2-oxonona-6,8-dienylphosphonate

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In ethyl acetate; for 3h; Reflux;
DOI:10.1055/s-0028-1083501

Reference yield: 94.0%

: 1108750-53-3
dimethyl (6E,8E)-9-(3,5-dimethoxyphenyl)-2-oxonona-6,8-dienylphosphonate

: 842103-98-4
tert-butyl (2-methyl-3-oxopropyl)carbamate

: 1234627-95-2
tert-butyl ((3Z,9E,11E)-12-(3,5-dimethoxyphenyl)-2-methyl-5-oxododeca-3,9,11-trien-1-yl)carbamate

: 1234627-91-8
tert-butyl (3E,9E,11E)-12-(3,5-dimethoxyphenyl)-2-methyl-5-oxododeca-3,9,11-trienylcarbamate

Guidance literature:: dimethyl (6E,8E)-9-(3,5-dimethoxyphenyl)-2-oxonona-6,8-dienylphosphonate; With N-ethyl-N,N-diisopropylamine; lithium chloride; In acetonitrile; at 20 ℃; for 0.5h; Inert atmosphere;

tert-butyl (2-methyl-3-oxopropyl)carbamate; In acetonitrile; for 16h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol101141a