benzyl<(2S,3S)-2,4-dihydroxy-3-<(phenylsulfonyl)amino>-1-butyl>methylsulfonium triflate

Base Information

Chemical Name:benzyl<(2S,3S)-2,4-dihydroxy-3-<(phenylsulfonyl)amino>-1-butyl>methylsulfonium triflate
CAS No.:119593-60-1
Molecular Formula:CF₃O₃S*C₁₈H₂₄NO₄S₂
Molecular Weight:531.595
Hs Code.:

Synonyms:benzyl<(2S,3S)-2,4-dihydroxy-3-<(phenylsulfonyl)amino>-1-butyl>methylsulfonium triflate

Suppliers and Price of benzyl<(2S,3S)-2,4-dihydroxy-3-<(phenylsulfonyl)amino>-1-butyl>methylsulfonium triflate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzyl<(2S,3S)-2,4-dihydroxy-3-<(phenylsulfonyl)amino>-1-butyl>methylsulfonium triflate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyl<(2S,3S)-2,4-dihydroxy-3-<(phenylsulfonyl)amino>-1-butyl>methylsulfonium triflate

There total 3 articles about benzyl<(2S,3S)-2,4-dihydroxy-3-<(phenylsulfonyl)amino>-1-butyl>methylsulfonium triflate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 17674-16-7
benzyl triflate

: 119593-58-7
(4S,5S)-5-<(phenylsulfonyl)amino>-2,2-dimethyl-4-<(methylthio)methyl>-1,3-dioxane

: 119593-60-1
benzyl<(2S,3S)-2,4-dihydroxy-3-<(phenylsulfonyl)amino>-1-butyl>methylsulfonium triflate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at -45 ℃; for 0.5h;
DOI:10.1021/jo00269a023

Reference yield:

: 119593-55-4,119593-56-5
(2RS,3S)-3-<(phenylsulfonyl)amino>-2,4-dihydroxy-1-(methylthio)butane

: 119593-60-1
benzyl<(2S,3S)-2,4-dihydroxy-3-<(phenylsulfonyl)amino>-1-butyl>methylsulfonium triflate

Guidance literature:: Multi-step reaction with 2 steps

1: toluenesulfonic acid / tetrahydrofuran / 3 h / Ambient temperature

2: 82 percent / Hunig's base / CH₂Cl₂ / 0.5 h / -45 °C

With o-toluenesulfonic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00269a023

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 119593-60-1
benzyl<(2S,3S)-2,4-dihydroxy-3-<(phenylsulfonyl)amino>-1-butyl>methylsulfonium triflate

Guidance literature:: Multi-step reaction with 2 steps

1: Hunig's base / CH₂Cl₂ / 0.25 h / -45 °C

2: 82 percent / Hunig's base / CH₂Cl₂ / 0.5 h / -45 °C

With N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1021/jo00269a023