4-(3,5-dioxo-10-oxa-4-azatricyclo[5.2.1.0^2,6]dec-8-en-4-yl)benzenesulfonylhydrazide

Base Information

• Chemical Name: 4-(3,5-dioxo-10-oxa-4-azatricyclo[5.2.1.0^2,6]dec-8-en-4-yl)benzenesulfonylhydrazide
• CAS No.: 114259-66-4
• Molecular Formula: C₁₄H₁₃N₃O₅S
• Molecular Weight: 335.34

Synonyms:4-(3,5-dioxo-10-oxa-4-azatricyclo[5.2.1.0^2,6]dec-8-en-4-yl)benzenesulfonylhydrazide

Chemical Property of 4-(3,5-dioxo-10-oxa-4-azatricyclo[5.2.1.0^2,6]dec-8-en-4-yl)benzenesulfonylhydrazide

Chemical Property:

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Technology Process of 4-(3,5-dioxo-10-oxa-4-azatricyclo[5.2.1.0^2,6]dec-8-en-4-yl)benzenesulfonylhydrazide

There total 2 articles about 4-(3,5-dioxo-10-oxa-4-azatricyclo[5.2.1.0^2,6]dec-8-en-4-yl)benzenesulfonylhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

4-(3,5-dioxo-10-oxa-4-azatricyclo[5.2.1.02,6]dec-8-en-4-yl)benzenesulfonyl chloride (114235-06-2) → 4-(3,5-dioxo-10-oxa-4-azatricyclo[5.2.1.02,6]dec-8-en-4-yl)benzenesulfonylhydrazide (114259-66-4)

Guidance literature:

With hydrazine hydrate; triethylamine; In methanol; for 5h; Ambient temperature;

Reference yield:

4-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)benzenesulfonyl chloride (36898-42-7) → 4-(3,5-dioxo-10-oxa-4-azatricyclo[5.2.1.02,6]dec-8-en-4-yl)benzenesulfonylhydrazide (114259-66-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 88 percent / diethyl ether

2: 63 percent / N₂H₄ / methanol

With hydrazine; In methanol; diethyl ether; 1: Diels-Alder reaction;

DOI:10.1080/00397910600941455

Reference yield: 79.0%

4-hydroxy-benzaldehyde (123-08-0,65581-83-1) + 4-(3,5-dioxo-10-oxa-4-azatricyclo[5.2.1.02,6]dec-8-en-4-yl)benzenesulfonylhydrazide (114259-66-4) → 4-(3,5-dioxo-10-oxa-4-azatricyclo[5.2.1.02,6]dec-8-en-4-yl)-N'-[(1E)-(4-hydroxyphenyl)methylene]benzenesulfonohydrazide

Guidance literature:

With hydrogenchloride; In ethanol; at 20 ℃; for 1h;

DOI:10.1080/00397910600941455

upstream raw materials:

4-(3,5-dioxo-10-oxa-4-azatricyclo[5.2.1.0^2,6]dec-8-en-4-yl)benzenesulfonyl chloride

4-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)benzenesulfonyl chloride

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