(R)-(+)-1-(3'-chlorophenyl)propyl acetate

Base Information

Chemical Name:(R)-(+)-1-(3'-chlorophenyl)propyl acetate
CAS No.:497165-73-8
Molecular Formula:C₁₁H₁₃ClO₂
Molecular Weight:212.676
Hs Code.:

Synonyms:(R)-(+)-1-(3'-chlorophenyl)propyl acetate

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Chemical Property of (R)-(+)-1-(3'-chlorophenyl)propyl acetate

Chemical Property:

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Technology Process of (R)-(+)-1-(3'-chlorophenyl)propyl acetate

There total 3 articles about (R)-(+)-1-(3'-chlorophenyl)propyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 108-05-4,9003-20-7
vinyl acetate

: 32019-30-0
(+/-)-1-(3'-chlorophenyl)propan-1-ol

: 32019-30-0,112777-67-0
(R)-1-(3-chlorophenyl)propan-1-ol

: 172748-80-0
(S)-1-(3-chlorophenyl)propan-1-ol

: 497165-73-8
(R)-(+)-1-(3'-chlorophenyl)propyl acetate

Guidance literature:: With lipase from Pseudomonas Cepacia; In various solvent(s); at 22 ℃; for 168h;
DOI:10.1016/S0957-4166(02)00415-9

Reference yield:

: 108-05-4,9003-20-7
vinyl acetate

: 32019-30-0
(+/-)-1-(3'-chlorophenyl)propan-1-ol

: 34841-35-5
3'-chloro-propiophenone

: 497165-73-8
(R)-(+)-1-(3'-chlorophenyl)propyl acetate

Guidance literature:: vinyl acetate; (+/-)-1-(3'-chlorophenyl)propan-1-ol; With lipase from Pseudomonas Cepacia; at 48 ℃; for 77h;

With manganese(IV) oxide; In dichloromethane; at 20 ℃;
DOI:10.1016/S0957-4166(02)00415-9

Reference yield:

: C₁₁H₁₁ClO₂

: (S)-1-(3-chlorophenyl)propyl acetate

: 497165-73-8
(R)-(+)-1-(3'-chlorophenyl)propyl acetate

Guidance literature:: With bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen; C₄₇H₄₁FeNO₂P₂; In 1,2-dichloro-ethane; tert-butyl alcohol; at 20 ℃; for 24h; under 15001.5 Torr; Overall yield = 26.4 mg; enantioselective reaction; Autoclave;
DOI:10.1016/j.tetlet.2020.152763